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Yes You Can Make Your Own TCT - If You Dare!
@Maya
Sartori in THE WAR GASES (q.v.) states that BrCN slowly polymerizes to cyanuric bromide, it ... |
23-5-2007 at 17:58
by: Sauron |
Help turning chloroform to formate.
You are trying to prepare normal alkyl formate esters like methyl formate, ethyl formate etc from ch ... |
23-5-2007 at 11:34
by: Sauron |
Yes You Can Make Your Own TCT - If You Dare!
I reiterate: formamide is just as irrelevant as formaldehyde, to cyanuric acid, isocyanuric acid, cy ... |
23-5-2007 at 09:49
by: Sauron |
Parr Stirred Pressure Reactors
On the pre-2004 Parr stirred reactors the motors are unsurprisingly 90V DC power from a 110V control ... |
23-5-2007 at 05:39
by: Sauron |
Australian power points
Wise move, gambler. You want something you can actually run an entire power strip off of, rather tha ... |
23-5-2007 at 02:42
by: Sauron |
Yes You Can Make Your Own TCT - If You Dare!
What leads you to conclude that cyanuric acid is a formaldehyde derivative?
Cyanuric acid is the ... |
23-5-2007 at 02:26
by: Sauron |
Lead Acetate distillation with PAA
If we limit this to the classical reagents SOCl2, PCL3, POCl3, PCl5 then I would concurr.
Howeve ... |
22-5-2007 at 23:57
by: Sauron |
Australian power points
@gambler
I haven't had time to look at that site yet, but I would recommend against the typical " ... |
21-5-2007 at 17:40
by: Sauron |
Australian power points
Forget about "power converters" as that nomenclature is used to describe small devices to power say, ... |
21-5-2007 at 04:31
by: Sauron |
Parr Stirred Pressure Reactors
There is a 4842 controller on LabX from a seller in UK called Rich-Monde but it is an older ad (not ... |
21-5-2007 at 02:29
by: Sauron |
Parr Stirred Pressure Reactors
There are times when glass just won't hack it. At such times an autoclave-type "bomb" reactor is the ... |
20-5-2007 at 21:22
by: Sauron |
Preparation of Isonicotinic Acid and Ethyl Isonotinate
The scheme for citric acid to citrazinic acid is on p.2 of the Potential Uses of Citric Acid thread ... |
20-5-2007 at 12:44
by: Sauron |
Potential uses of Citric Acid
The rxn of ammonia with methyl or ethyl citrate to give citrazinic acid was popular in the first hal ... |
20-5-2007 at 12:39
by: Sauron |
keten lamp
And I am still waiting for vinyl acetate to arrive. I think it may take substantial experimentation ... |
20-5-2007 at 00:36
by: Sauron |
Synthesis of Sulfur Trioxide and Oleum: The persulfate method
@G C
Nice thread! SO3 is always of interest. The procedure you have described looks like a simpl ... |
18-5-2007 at 12:02
by: Sauron |
Call for discussion of several methods of producing pyruvic acid by dry distillation
Oh true enough. Still, you would idly light your Zippo (now a fashionable antique cigarette lighter. ... |
17-5-2007 at 07:42
by: Sauron |
Call for discussion of several methods of producing pyruvic acid by dry distillation
I doubt I'd use peanut oil if distilling oxidizing liquids. Silicone oil, on the other hand, is pret ... |
17-5-2007 at 07:21
by: Sauron |
Call for discussion of several methods of producing pyruvic acid by dry distillation
Fine. You use a free flame in the lab. Go right ahead. Be my guest. Meanwhile I'll buy some marshmel ... |
16-5-2007 at 19:08
by: Sauron |
Call for discussion of several methods of producing pyruvic acid by dry distillation
An airbath like the Kugelrohr oven for the old 4 liter model that is no longer made would be good. n ... |
16-5-2007 at 03:14
by: Sauron |
Bird Flu ??
Those might be useful for poultry workers or people who live near poultry farms or ar otherwise at r ... |
15-5-2007 at 20:35
by: Sauron |
Call for discussion of several methods of producing pyruvic acid by dry distillation
@matchheads:
Right. Free flames in the lab. I guess you don't work much with ether, CS2, THF, met ... |
15-5-2007 at 20:04
by: Sauron |
PUBLIC ADVISORY: Pictures
Sorry, renown is correct. No such word as 'reknown' exists in the English language. If you think oth ... |
15-5-2007 at 19:42
by: Sauron |
Bird Flu ??
It's a big problem still.
If you are a bird.
It's a nonzero risk if you are a poultry worker b ... |
15-5-2007 at 12:53
by: Sauron |
Call for discussion of several methods of producing pyruvic acid by dry distillation
Often with a foaming problem like this you can handle it by switching from the 3L flask specified to ... |
15-5-2007 at 12:43
by: Sauron |
Call for discussion of several methods of producing pyruvic acid by dry distillation
It's repetitious to include the Vogel procedure which he simply downsized a little from the Org.Syn. ... |
15-5-2007 at 10:14
by: Sauron |
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