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Toluene For Hydrogenation Reaction
I am going to start a hydrogenation reaction, but I just hit one problem. Does palladium on carbon i ...
7-3-2021 at 09:55
by: Triflic Acid
OTC Amine protection?
Oh, I got that synthesis from Ullmann's Encyclopedia of Industrial Chemistry. On page ten of the sec ...
4-3-2021 at 08:30
by: Triflic Acid
OTC Amine protection?
Have you looked into the TosCl? That can be made pretty easily from toluene and sulfurly chloride(su ...
2-3-2021 at 07:29
by: Triflic Acid
Separation of dimethylcarbonate from 1,3 dioxolane
They gave decently different boiling points, 90C for the dimethyl carbonate and 75C for the dioxolan ...
1-3-2021 at 10:15
by: Triflic Acid
Question about pressure
I can't help but ask, what reaction are you planning to do with this reactor? If are doing something ...
26-2-2021 at 07:28
by: Triflic Acid
OTC Oxalyl Chloride?
If you won't but a rubber stopper in it, how about a all natural cork :P. Nobody has answered my que ...
22-2-2021 at 11:39
by: Triflic Acid
OTC Oxalyl Chloride?
I do have access to t-butanol. I was just showing how t-butanol could be made to make this a fully O ...
22-2-2021 at 10:36
by: Triflic Acid
OTC Oxalyl Chloride?
What would be a better substrate?


[Edit: Second Question: Is there another acid chloride that ...
22-2-2021 at 10:26
by: Triflic Acid
OTC Oxalyl Chloride?
@ clearly not atara, I didn't think about the danger of phosgene production. That scares me out of t ...
22-2-2021 at 10:13
by: Triflic Acid
OTC Oxalyl Chloride?
It says on organic chemistry portal that tert-butyl hypochlorite reacts with aldehydes to form acid ...
22-2-2021 at 07:30
by: Triflic Acid
Chemical Reactions for Beginner Chemist
With what you have/ are going to buy, I can see only one good project. Make HCN :P But seriously, yo ...
11-2-2021 at 07:27
by: Triflic Acid
Any way to tell if there is bromobenzene in benzene?
All of these ideas fall short in one small place, I can't open the reaction flask during the reactio ...
9-2-2021 at 22:17
by: Triflic Acid
A new way to make NCl3?
I was just thinking that, if you bubbled chlorine through liquid ammonia, wouldn't you get NCl3. And ...
8-2-2021 at 22:23
by: Triflic Acid
Any way to tell if there is bromobenzene in benzene?
I think that at this point, I'm just going to say to hell with it and run the reaction until I don't ...
6-2-2021 at 22:29
by: Triflic Acid
Mechanism help. (Acetanilide)
For this reaction, you really have two options. Either you don't use triethylamine, and create hydro ...
5-2-2021 at 11:14
by: Triflic Acid
Any way to tell if there is bromobenzene in benzene?
Or, even better, I could just track the amount of hydrogen consumed.
5-2-2021 at 11:05
by: Triflic Acid
Any way to tell if there is bromobenzene in benzene?
On another note, is it possible to track the amount of precipitate that forms, if I put triethylamin ...
5-2-2021 at 10:53
by: Triflic Acid
Any way to tell if there is bromobenzene in benzene?
I am working on something where I am trying to hydrogenated aryl bromides to get arenes. If I want t ...
3-2-2021 at 18:54
by: Triflic Acid
Deprotonated alkyne stability
I might just be bad at searching the internet, but I can't find a single source about these metal ph ...
30-1-2021 at 13:02
by: Triflic Acid
Disulfur diiodide substitute for phosphorus triiodide
I was actually thinking of the alcohol as the solvent, and the sulfur as a suspension that forms som ...
29-1-2021 at 10:17
by: Triflic Acid
Deprotonated alkyne stability
So, if I wanted to make a whole bunch of these, I would have to add anhydrous metal salts to sodium ...
27-1-2021 at 12:52
by: Triflic Acid
Disulfur diiodide substitute for phosphorus triiodide
I was thinking that adding idodine to sulfur would form the sulfur iodide in situ, like when you pas ...
27-1-2021 at 12:49
by: Triflic Acid
Disulfur diiodide substitute for phosphorus triiodide
I want to make akyl iodides from alcohols. Mainly methyl iodide. I don't have phosphorus, so I start ...
26-1-2021 at 22:25
by: Triflic Acid
Deprotonated alkyne stability
Just a question, but does adding phenylacetylene to a metal nitrate always give the phenylactylenide ...
26-1-2021 at 22:17
by: Triflic Acid
Deprotonated alkyne stability
Well, photosensitive is expected with silver, but the fact that it is water stable is good. Also, is ...
24-1-2021 at 19:07
by: Triflic Acid
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