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Hypothetically drinkable ethanol from methylated spirits
No, I did not try the rxn with ethylenebromide. I simply didn't want to contaminate the ethanol with ...
6-8-2019 at 05:34
by: Pumukli
Hydrazine
Congrats for the synth!

I'd like to second Boffis' amazement on omitting gelatine. My exact thoug ...
6-8-2019 at 05:28
by: Pumukli
Cinnamic Acid from Benzaldehyde and Acetic Acid?
Sounds plausible, though not at 16 Celsius but at 160 Celsius, in a sealed tube!
1-8-2019 at 05:48
by: Pumukli
Substitution of Magnesium Methoxide for Sodium Methoxide
My attempt to substitute NaOMe with Mg(OMe)[sub]2[/sub] in a condensation reaction became a failure. ...
31-7-2019 at 12:28
by: Pumukli
A long and hard quest, can anyone help me?
As j_sum1 said: "let us know what what you have been studying"!

What can be the F gas which react ...
28-7-2019 at 04:07
by: Pumukli
m-xylene, 2,6-xylidine and lidocaine
What would you like to do with lidocaine? Do you intend to actually use it as lidocaine is used, as ...
27-7-2019 at 11:30
by: Pumukli
Anhydrous AlCl3
First route is unknown for me. On paper, yes, but in practice how to remove the water? Refluxing wit ...
27-7-2019 at 11:10
by: Pumukli
The Short Questions Thread (4)
2-ethylhexanol why should it be brown? It is a simple aliphatic alcohol of which the C-chain isn't t ...
26-7-2019 at 20:01
by: Pumukli
Why is my zinc powder not powder???
Powder = big surface area = fast oxidation.

My zinc powder also contains bigger "chunks" and very ...
24-7-2019 at 05:05
by: Pumukli
2,3-dimethyl-2-butene chemistry
I don't know much about olefines but I can tell you that last year when I was preparing my cyclohexe ...
23-7-2019 at 11:01
by: Pumukli
The most useful three things in my lab
j_sum1: not boring, because I also need a good dishwasher/someone/as a last resort me to do the wash ...
23-7-2019 at 10:49
by: Pumukli
The most useful three things in my lab
I thought I'd start this thread on the most useful equipments we use. I'd like to hear about YOUR mo ...
22-7-2019 at 02:52
by: Pumukli
Anthranilic acid fail
I slowly explore parts of this particular Hofmann rearrangement and I found it more and more interes ...
21-7-2019 at 09:50
by: Pumukli
Reaction dynamics of thiosulfate ion
Maybe the slowest step is the aggregation of BaS[sub]2[/sub]O[sub]3[/sub] miniature (nanometer range ...
20-7-2019 at 00:36
by: Pumukli
4-chlorocinnamic acid synthesis without distillation
Nice synth!

I'm curious whether the product has pleasant smell or not. :)
18-7-2019 at 11:16
by: Pumukli
Mass and Weight
Good subject, Sulaiman!

I'd urge all our members if they want to do chemistry on a bit more serio ...
18-7-2019 at 05:18
by: Pumukli
Nitration and acetone
Isn't formic acid oxidized further immediately? (CO[sub]2[/sub], H[sub]2[/sub]O, more heat)

18-7-2019 at 02:55
by: Pumukli
Anthranilic acid fail
Thanks Amos, good to know that "cocoa powder" from this reaction is still as good as the original th ...
17-7-2019 at 11:37
by: Pumukli
Anthranilic acid fail
If there was an "Analytical Chemistry" subsection on this board then I were posting this there:

I ...
14-7-2019 at 11:54
by: Pumukli
Anthranilic acid fail
The "everyielding crystal source" deposited ridiculous ammounts of tan/light brown crystalls during ...
13-7-2019 at 01:22
by: Pumukli
Future-gazing: available now, restricted tomorrow?
No need to defend bleach makers! For decades, regular bleach was 5.25% (0.7 M or what) and it was no ...
12-7-2019 at 12:58
by: Pumukli
Vacuum Oven vs Kiln for Molecular Sieve Drying
Isn't it dangerous to put a few litres of wet sieves into a regular oven at high heat? I mean explos ...
11-7-2019 at 08:13
by: Pumukli
Future-gazing: available now, restricted tomorrow?
I think something happened. There was (still is) a shop, real and online as well, which stocked 96% ...
9-7-2019 at 12:57
by: Pumukli
Anthranilic acid fail
To continue my monologue I burned a sample of the powder at the tip of the blade of a thin knife. Ye ...
9-7-2019 at 06:53
by: Pumukli
Anthranilic acid fail
I was wondering that maybe what I got is the calcium salt of AA as a precipitate. (Because I used Ca ...
8-7-2019 at 23:49
by: Pumukli
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