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2,5-dimethoxy-4-iodo-beta-nitrostyrene
[rquote=322473&tid=23916&author=Methyl.Magic]Hi, Red-Al causes dehalogenation for sure.[/rqu ...
15-3-2014 at 03:23
by: Nicodem
What is the hydride molar requirement to reduce nitro compounds?
[rquote=322694&tid=29469&author=Electra]I cannot calculate the stichiometry if I do not know ...
15-3-2014 at 01:19
by: Nicodem
What is the hydride molar requirement to reduce nitro compounds?
You can easily calculate the stoichiometry of the redox reactions, if you count the exchanged electr ...
14-3-2014 at 08:58
by: Nicodem
Copper Cyanurate > mystery compound?
[rquote=322613&tid=29474&author=numos]Ok... So I saw this substance mentioned in various pos ...
14-3-2014 at 08:37
by: Nicodem
What conditions favor dehydration of aldol condensation products?
[rquote=321893&tid=29379&author=FireLion3]What is it that favors the dehydration of nitroalc ...
11-3-2014 at 10:43
by: Nicodem
A question about a reaction involving translocation of carbonyl group of a ketone
[rquote=321565&tid=29309&author=kmno4]There is an article titeled "[i]Transposition of Keton ...
6-3-2014 at 08:56
by: Nicodem
A question about a reaction involving translocation of carbonyl group of a ketone
[rquote=321560&tid=29309&author=forgottenpassword]With the reagents specified I can only fin ...
5-3-2014 at 12:34
by: Nicodem
Lewis acids: SnCl4 and SbCl5
I found no specific example of SnCl[sub]4[/sub] catalyzed alkylation of benzene or toluene with [sup ...
5-3-2014 at 10:24
by: Nicodem
A question about a reaction involving translocation of carbonyl group of a ketone
Claus, this is no "translocation of carbonyl group of a ketone". The carbonyl group does not translo ...
5-3-2014 at 09:34
by: Nicodem
Lewis acids: SnCl4 and SbCl5
[rquote=321064&tid=29238&author=blogfast25]That's because I'm looking for an example of a re ...
4-3-2014 at 09:45
by: Nicodem
1-dimethylamino-2-chloropropane
You cannot analyze rapidly inter-convertible compounds by GC - that's quite obvious.

You could po ...
2-3-2014 at 01:31
by: Nicodem
Lewis acids: SnCl4 and SbCl5
SnCl[sub]4[/sub] is a commonly used acid catalyst for Friedel-Crafts acylations (if you check the li ...
1-3-2014 at 11:00
by: Nicodem
prep of HCl in isoOH?
[quote]I may try again now that I'm working with purified phenethylamine freebase, but previous atte ...
20-2-2014 at 12:43
by: Nicodem
NMR purity analysis...?
NMR can not be used to measure purity. Purity can only be measured by developing a method specific f ...
20-2-2014 at 08:31
by: Nicodem
What determines the reduction of nitro groups to ketones over amines, or vice versa
[rquote=319795&tid=28616&author=Electra]Though I still do not see my quesiton answered.[/rqu ...
20-2-2014 at 08:15
by: Nicodem
prep of HCl in isoOH?
Ask yourself why do you even need anhydrous HCl in isopropanol? If your goal is to only make an amin ...
20-2-2014 at 07:52
by: Nicodem
Aniline
[rquote=318092&tid=28847&author=SM2]Short of the classical reduction of 1-nitrobenzene, I've ...
7-2-2014 at 05:53
by: Nicodem
Copper(II) Aspirinate Synthesis
[rquote=318198&tid=9920&author=sargent1015]Didn't think about it, but here is the wiki answe ...
7-2-2014 at 04:45
by: Nicodem
too many posts sent to detritus
[rquote=317173&tid=28340&author=Zyklonb]I wasn't planning on mentioning this, but before I c ...
30-1-2014 at 06:52
by: Nicodem
Pd/H2 reduces aldehydes to alkanes or alcohols?
[rquote=316879&tid=28729&author=FireLion3]We can use the example above. In the case of a ben ...
28-1-2014 at 11:05
by: Nicodem
Reaction of halogen ketones with ammonia
[rquote=316917&tid=28730&author=confused]The rection should be something like this[/rquote]
...
28-1-2014 at 10:40
by: Nicodem
troubleshooting microwave synthesis of melatonin.
The remarkable similarity of that route to the classical Japp-Klingemann reaction and the non-sense ...
22-1-2014 at 08:15
by: Nicodem
troubleshooting microwave synthesis of melatonin.
[rquote=316259&tid=28630&author=melatonin]I'm trying to do a synthesis of 5 methoxy tryptami ...
22-1-2014 at 06:47
by: Nicodem
What determines the reduction of nitro groups to ketones over amines, or vice versa
[rquote=316219&tid=28616&author=Electra]What really puzzles me is that I have seen different ...
22-1-2014 at 06:15
by: Nicodem
Photoreaction of Br2 and Benzoyl peroxide?
[rquote=316078&tid=28596&author=swintarka]I was wondering if mixture of Br2 and benzoyl pero ...
20-1-2014 at 11:15
by: Nicodem
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