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Pyruvic acid synthesis?
With all the posts on acetone chlorination with TCCA on this forum, you just have to bring out chlor ...
15-3-2007 at 10:51
by: Nicodem
Indole-3-Carbinol Oxidation
[url=http://v3.espacenet.com/textdoc?DB=EPODOC&IDX=EP0658533&F=0&QPN=EP0658533]EP658533[ ...
15-3-2007 at 10:43
by: Nicodem
Preparing Na2S2O8
Where I live it can be found in just about any pool section of large stores.
Due to Klute, I have r ...
14-3-2007 at 13:36
by: Nicodem
now for some retrosynthesis: 3-[N-diethyl-1-(n-propanamide)] on a primary nitrogen.
http://www.diss.fu-berlin.de/2004/81/index.html
http://molpharm.aspetjournals.org/cgi/content/abstr ...
14-3-2007 at 13:13
by: Nicodem
now for some retrosynthesis: 3-[N-diethyl-1-(n-propanamide)] on a primary nitrogen.
According to the literature you are lucky in that:
a.) acrylamides are just electrophilic enough fo ...
14-3-2007 at 12:04
by: Nicodem
synthesis of n-propyl-p-nitrophenylamine
Try using 3 equivalents of propylamine instead of K2CO3 as acid scavenger, methanol or ethanol as so ...
14-3-2007 at 10:54
by: Nicodem
now for some retrosynthesis: 3-[N-diethyl-1-(n-propanamide)] on a primary nitrogen.
[quote][i]Originally posted by stoichiometric_steve[/i]
QSAR studies say that an amphetamine like D ...
13-3-2007 at 14:13
by: Nicodem
Preparing Na2S2O8
Rather buy Oxone. I can't imagine a reaction where Na2S2O8 can not be replaced by it.
12-3-2007 at 11:25
by: Nicodem
benzylnitrile
[quote][i]Originally posted by garage chemist[/i]
In the "theoretical amphetamine variants" thread, ...
12-3-2007 at 11:17
by: Nicodem
Primary Amine metathesis
[quote][i]Originally posted by franklyn[/i]
[color=red][size=4][b]3 )[/b][/size][/color]

Halog ...
11-3-2007 at 12:20
by: Nicodem
What to do with diphenyl carbonate?
You better stick to the workup that I suggested earlier. The one that you suggested will not give yo ...
9-3-2007 at 08:56
by: Nicodem
theoretical amphetamine variants
Well, here we go with another potential empathogen, 1-(indol-6-yl)isopropylamine:
[i]Pharmacology r ...
8-3-2007 at 12:23
by: Nicodem
What to do with diphenyl carbonate?
Chemical degradation half lives are values true only for monophasic systems. If you have a mixture o ...
8-3-2007 at 11:49
by: Nicodem
What to do with diphenyl carbonate?
You can not have phenol there after you used excess NaOH for the hydrolysis. Utmost you have a mixtu ...
4-3-2007 at 04:01
by: Nicodem
Names of dicarboxylic acids
[quote][i]Originally posted by 12AX7[/i]
Speaking of carboxylic acids, what is (if it exists) C(COO ...
3-3-2007 at 10:06
by: Nicodem
theoretical amphetamine variants
Such bicyclic systems where the ethylamine side chain is rotationally restricted by being incorporat ...
3-3-2007 at 02:26
by: Nicodem
KI + HCl --> Lugol's iodine??
Your knowledge of chemistry is awesome! I'm left speechless.
3-3-2007 at 01:12
by: Nicodem
I want some cyanide to play with!
[quote][i]Originally posted by DeAdFX[/i]
So I assume you were wanting to synthesize Acetone nitril ...
3-3-2007 at 01:08
by: Nicodem
Hydroxylamine NH2OH Uses (and Production)
Don't trust Wikipedia on such things. Bisulphites are in my opinion unable to reduce the nitrate ani ...
3-3-2007 at 00:54
by: Nicodem
Equivalence
If an equivalent is called for, then it is meant as equivalent according to the reaction stoichiomet ...
3-3-2007 at 00:25
by: Nicodem
theoretical amphetamine variants
[quote][i]Originally posted by jon[/i]
mirapex is a benzothiazole derivitive of amphetamine[/quote] ...
3-3-2007 at 00:15
by: Nicodem
Purification of 1-bromobutane
Concentrated H2SO4 is just fine for primary alcohols. It will not oxidize the bromide as it gets dil ...
1-3-2007 at 15:07
by: Nicodem
Purification of 1-bromobutane
The yellow color is not from bromine but from side products. You need to distill it or else you can ...
27-2-2007 at 11:29
by: Nicodem
Super toxin?
That "toxic lady" story was a hoax set up by the hospital in order to hide the reason why the pacien ...
27-2-2007 at 11:18
by: Nicodem
preparation of triethylamine hydrochloride in laboratory
[quote][i]Originally posted by LoKi[/i]
Thats funny, I was just pondering how to make triethylamine ...
27-2-2007 at 11:10
by: Nicodem
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