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Acetonitrile form Ammonium acetate
Well there is no one method but OrgSyn has this for Nicotinonitrile which could be adapted. It's one ... |
11-11-2008 at 15:29
by: panziandi |
3-chlorophenol, 3-chloroaniline
I would imagine you would start with (benzene and nitrate it to nitrobenzene) nitrobenzene, chlorina ... |
11-11-2008 at 15:17
by: panziandi |
Acetonitrile form Ammonium acetate
Haha... but if you have P2O5 you may as well just use that to dehydrate! But I suppsoe that is your ... |
9-11-2008 at 11:36
by: panziandi |
Acetonitrile form Ammonium acetate
I would make sure the polyphosphoric acid is anhydrous by heating it under a vacuum for some time an ... |
9-11-2008 at 11:22
by: panziandi |
Uranyl Acetate and Nitrate?
I believe it would be best to ship it as you would ship mercury, lead, thallium, cadmium compounds. ... |
8-11-2008 at 10:44
by: panziandi |
Chlorination of CS2 Revisited
POCl3 doncha mean Sauron? :p ... |
3-11-2008 at 05:42
by: panziandi |
Inorganic Phosphorus Transformations
Indeed activity of the AC depends on particle size, metal ion contamination, etc. Perhaps it would b ... |
1-11-2008 at 15:13
by: panziandi |
Inorganic Phosphorus Transformations
I would expect most of what is formed to be hydrogen chloride and sodium phosphate :s.
Perhaps re ... |
1-11-2008 at 13:08
by: panziandi |
Chlorination of CS2 Revisited
I'm jealous of some of your equipment and chemicals Sauron... it woirks both ways :p!
Ah ok! I su ... |
1-11-2008 at 12:56
by: panziandi |
Inorganic Phosphorus Transformations
I see! Well yes it is water reactive, toxic gas releasing, dangerous to the environment chemicals LO ... |
1-11-2008 at 10:51
by: panziandi |
Inorganic Phosphorus Transformations
http://www.sigmaaldrich.com/catalog/search/ProductDetail/ALDRICH/400971
http://www.sigmaaldrich.c ... |
1-11-2008 at 10:30
by: panziandi |
Inorganic Phosphorus Transformations
Something like BASF perhaps. It's more of an industrial chemical than a lab reagent, well apart form ... |
1-11-2008 at 09:53
by: panziandi |
Chlorination of CS2 Revisited
Good I expected you to know how to handle CS2!
I have no problem really getting hold of CHCl3 and ... |
1-11-2008 at 08:13
by: panziandi |
Inorganic Phosphorus Transformations
I have 2 x 500g of Zn3P2 from BDH but alas I tried looking it up on VWR.com and all I found was smal ... |
1-11-2008 at 08:03
by: panziandi |
Chlorination of CS2 Revisited
Well, I suggest UV &/or peroxide induced free radical chlorination of CH2Cl2 using Cl2. For exam ... |
31-10-2008 at 16:38
by: panziandi |
Chlorination of CS2 Revisited
Well I PCl5 will not chlorinate DCM AFAIK. ICl will halogenate DCM via radical reaction to form iodo ... |
31-10-2008 at 15:01
by: panziandi |
Chlorination of CS2 Revisited
I hate to say it but all the time spent trying to find a high yielding "easy" and "economical" metho ... |
31-10-2008 at 13:48
by: panziandi |
sourceachem (UK)
Old source, repacks labpak and also over counter chemicals from a pharmacy. Adds a huge % to all the ... |
24-10-2008 at 15:48
by: panziandi |
birdshot sodium
Indeed but sometimes when you want an exact weight of metal or hydride it is necessary to remove the ... |
24-10-2008 at 13:11
by: panziandi |
"Who-me?"
Not familiar myself I'm affraid but many sulphur compounds stink. Wiki says implies it was a blend o ... |
23-10-2008 at 14:30
by: panziandi |
birdshot sodium
It takes a bit of skill or time experimenting to find the correct way to get the suitable sized part ... |
23-10-2008 at 12:37
by: panziandi |
birdshot sodium
Sure! Basically you want to obtain a two-necked flask and dual manifold (vacuum and inert gas). Weig ... |
22-10-2008 at 12:02
by: panziandi |
Fluoromethanes and fluoro-halomethanes
Yes I stumbled upon that synthesis too.
I didn't know it was violently reactive with metals at r ... |
21-10-2008 at 14:02
by: panziandi |
Sources of Conc. H2SO4 in the United Kingdom (England)
Indeed LP sells alot of chemicals to the public in the UK and are very cheap. I used to use some dra ... |
21-10-2008 at 13:38
by: panziandi |
birdshot sodium
Not terribly long since xylene will wet which will obviously lead to reaction with sodium and it'll ... |
21-10-2008 at 13:06
by: panziandi |
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