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A Sad Day - Another Great Supplier Gone - Elemental Scientific
Another one I like ordering from is https://www.amazon.com/stores/Alliance+Chemical/page/32AD3F07-2B ...
29-3-2021 at 06:12
by: Triflic Acid
Method for demethylation of secondary amine?
Maybe you could kill both the secondary amines to primary amines, and use a bulky methylating agent ...
27-3-2021 at 12:50
by: Triflic Acid
calcium benzoate dry distillation safety
Low side just means that it is a rather small value and the yield is not very good.
27-3-2021 at 12:45
by: Triflic Acid
New catalysis for conversation of methane to methanol
In my universities lab, I'm going to be working on a direct oxidation of hexane to adipic acid in a ...
26-3-2021 at 11:20
by: Triflic Acid
Oxalyl Chloride Challenge
Oh, when he said decomposition, I immediately thought that he was doing something around pyrolysis. ...
25-3-2021 at 12:20
by: Triflic Acid
Oxalyl Chloride Challenge
And, how are you going to deal with that nice chlorinated decomposition product COCl2, commonly call ...
25-3-2021 at 06:30
by: Triflic Acid
How to balance tall glassware
Thanks for everyones help. I settled on the idea of a hood latice, and began building yesterday. I'l ...
22-3-2021 at 06:37
by: Triflic Acid
How to balance tall glassware
How make I do that @j_sum1? Could you send a photo? When I googled it, I could only find test tube r ...
21-3-2021 at 08:16
by: Triflic Acid
How to balance tall glassware
I have an experiment that uses a leigbeg condenser. This particular condenser is more than a foot ta ...
20-3-2021 at 21:30
by: Triflic Acid
Making Boron Triiodide
I was also doubtful that it work, (the methyl iodide and the boron triiodide both). But still, no ha ...
17-3-2021 at 16:06
by: Triflic Acid
Making Boron Triiodide
One random thing, but, for methyl iodide, couldn't one do a finkelstein type reaction where an insol ...
17-3-2021 at 11:56
by: Triflic Acid
Making Boron Triiodide
On Wikipedia it says: Boron triiodide can be prepared by the reaction of boron with iodine at 209.5 ...
17-3-2021 at 10:35
by: Triflic Acid
Making Boron Triiodide
Can I make boron triiodide in situ, by combining iodine, boron, and a free radical initiator(like UV ...
17-3-2021 at 09:33
by: Triflic Acid
Reaction of sulfur chlorides with alcohols
I am trying to find some sort of literature that outlines the reaction of sulfur chlorides with alco ...
15-3-2021 at 18:46
by: Triflic Acid
Synthesis of N-methylimidazole
Just out of curiosity, did you find that in a prep? If so, could you give a link or something?
15-3-2021 at 17:28
by: Triflic Acid
Synthesis of N-methylimidazole
I have imidazole, and am going to make N-methylimidazole by reacting it with MeI and then NaOH. What ...
15-3-2021 at 16:11
by: Triflic Acid
phosphorus oxychloride (POCl3)
I'm not too sure about this, but maybe reacting something like SOCl2, which has been prepared on the ...
15-3-2021 at 12:06
by: Triflic Acid
How to store methyl iodide
First the neighbors heard a blower fan coming from the garage, then they see me burying something in ...
15-3-2021 at 11:58
by: Triflic Acid
How to store methyl iodide
Ok, in that case, I'll use the MeI within a few days (< 1 week) for the first step in an ionic li ...
15-3-2021 at 11:22
by: Triflic Acid
How to store methyl iodide
Right now, it's still pretty cold here, with highs in the 50s or 60s (F, not C :P).
15-3-2021 at 11:12
by: Triflic Acid
How to store methyl iodide
The forum has a bunch on things about making methyl iodide, but practically nothing about storing it ...
15-3-2021 at 10:51
by: Triflic Acid
Disulfur diiodide substitute for phosphorus triiodide
I am planning on running this experiment, but I can't find a single paper outlining the reaction of ...
14-3-2021 at 20:55
by: Triflic Acid
1-pentylnaphthalene theory
Maybe first sulfonate the aromatic at high temp, to get 2 napthalene sulfonic acid, thats a meta dir ...
10-3-2021 at 07:27
by: Triflic Acid
Toluene For Hydrogenation Reaction
Thanks for that, I am not conducting the reaction in air, only the workup.
7-3-2021 at 13:09
by: Triflic Acid
How many water's of hydration does triethylammonium bromide have?
I am doing something where I need to measure the number of moles of solid triethylammonium bromide, ...
7-3-2021 at 10:05
by: Triflic Acid
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