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NHN synthesis not working
When you are dissolving nickel metal in nitric acid, you need to use much more acid (or less of the ...
13-12-2021 at 09:11
by: Microtek
Quantitative NHN synthesis without Hydrazine hydrate
I know what hydrogen peroxide is, I just think that the correct term has been lost in translation. I ...
10-12-2021 at 06:09
by: Microtek
Quantitative NHN synthesis without Hydrazine hydrate
I think the "oxygenated water" is hydrogen peroxide. I found that US6605265 is very similar to what ...
9-12-2021 at 08:35
by: Microtek
Quantitative NHN synthesis without Hydrazine hydrate
If you are going to freebase the hydrazine anyway, what's the point of converting it to the chloride ...
6-12-2021 at 01:36
by: Microtek
New Energetic Materials - Current Research
I'm fairly certain that metathesis won't work to produce urazine perchlorate. The urazine is a very ...
26-11-2021 at 02:10
by: Microtek
New Energetic Materials - Current Research
That is a predicted value using the ACDlabs software. ACDlabs is notorious for overestimating the de ...
24-11-2021 at 23:10
by: Microtek
New Energetic Materials - Current Research
I'm in the EU, and haven't been able to find carbohydrazide locally. Importing from outside the EU i ...
24-11-2021 at 02:02
by: Microtek
New Energetic Materials - Current Research
Ok, so I've synthesized what I believe to be urazine.

I began from dimethylcarbonate and followe ...
23-11-2021 at 07:26
by: Microtek
Short question / quick answer - Thread
Hydrazine sulfate is not very soluble in ethanol. I suggest you use 1 mol HS to one mol sodium hydro ...
21-11-2021 at 03:11
by: Microtek
Effects of Various Binders on PBX Composition Performance
Exactly. I still think it is possible to produce a more conventional charge geometry using the metho ...
18-11-2021 at 23:51
by: Microtek
Effects of Various Binders on PBX Composition Performance
Latex can work as a binder, but not as a plasticizer. From the context in which you use the term, I ...
17-11-2021 at 06:43
by: Microtek
Effects of Various Binders on PBX Composition Performance
1:9 is correct for the cheddite you mentioned, it's just not very moldable. If you increase the vase ...
16-11-2021 at 04:32
by: Microtek
Erythritol Tetranitrate
Yes, that works too. Be aware, however, that the viscosity of such a nitrating mixture is much highe ...
15-11-2021 at 23:33
by: Microtek
Effects of Various Binders on PBX Composition Performance
The purpose of the vaseline jelly in the chlorate mixes is mainly to act as a fuel. The plasticity i ...
15-11-2021 at 08:43
by: Microtek
Erythritol Tetranitrate
Ok, I see now. If you can find a glass rod of suitable diameter, you can use that for plugging the t ...
15-11-2021 at 02:12
by: Microtek
Erythritol Tetranitrate
A couple of points:

- As Katyusha said, the Al-foil should be used as insulation by wrapping it l ...
14-11-2021 at 09:48
by: Microtek
New Energetic Materials - Current Research
Well, my charges are rarely more than 1 gram secondary (hence my moniker), so a potential accident w ...
12-11-2021 at 14:15
by: Microtek
Smokeless Rocket Propellant
You could take a look here:

[url=http://www.thrustgear.com/topics/Kn_Notes.htm]http://www.thrustg ...
10-11-2021 at 09:11
by: Microtek
ETN Stability as primary explosive
You should only aim for pH 7-7.5 otherwise you risk hydrolysis or other reactions (if you go to high ...
4-11-2021 at 13:58
by: Microtek
ETN Stability as primary explosive
I would suggest you do this instead for recrystallizing:

- Dissolve in acetone

- Add solid bic ...
4-11-2021 at 02:57
by: Microtek
New Energetic Materials - Current Research
PETN has an impact sensitivity of 3.6J, mannitol hexanitrate 0.8-1.8 J. I couldn't find data for ETN ...
29-10-2021 at 10:05
by: Microtek
New Energetic Materials - Current Research
Good find, that makes it much more OTC (I had forgotten all about that experiment). For those of us ...
28-10-2021 at 23:01
by: Microtek
New Energetic Materials - Current Research
@katyushaslab

I did see that entry in Ullmann, but everywhere else I have looked, people are diet ...
28-10-2021 at 07:48
by: Microtek
New Energetic Materials - Current Research
During a bout of research, I stumbled on this paper by Klapƶtke:

[url=https://chemistry-europe.o ...
25-10-2021 at 06:14
by: Microtek
(not) RDX from hexamine and mixed acids?
What is the precipitate insoluble in? Water? Or the supernatant? If the latter is the case, the crys ...
25-10-2021 at 03:34
by: Microtek
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