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Alexander Shulgin Books
That's admirably tolerant.
24-9-2007 at 10:30
by: Sauron
Erratum in Saunders "Phosphorus and Fluorine"
Hmmm. Organophosphorous compounds are mostly pretty nasty even when they aren't military grade. The ...
24-9-2007 at 10:27
by: Sauron
Alexander Shulgin Books
My reputation and image are intact. Yours are IMO shot to shit. I encourage a lot of people on this ...
24-9-2007 at 10:04
by: Sauron
Erratum in Saunders "Phosphorus and Fluorine"
The book is in the forum library, freely downloadable pdf.

There are several systems of phosphoru ...
24-9-2007 at 09:51
by: Sauron
Trialkyl Phosphites from Alkoxide and PBr3?
I would not willingly work with WP. Did it once long ago and survived to tell the tale.

A series ...
24-9-2007 at 09:40
by: Sauron
Alexander Shulgin Books
You do not need to apologize to anyone for being an amateur.

However, since you did say you are i ...
24-9-2007 at 09:00
by: Sauron
Trialkyl Phosphites from Alkoxide and PBr3?
Saunders et al used SbF3 to fluorinate PCl3 and POCl3 to PCl2F abd POCl2F, but yields were lousy (,3 ...
24-9-2007 at 08:52
by: Sauron
Sartori Supplement to The War Gases
Mario Sartori's classic The War Gases graces the forum library so some of you may like to know that ...
24-9-2007 at 08:39
by: Sauron
Alexander Shulgin Books
That's right. You're a one man Eli Lilly & Co.

So let us know when Elvis gets here.

Look, ...
24-9-2007 at 08:17
by: Sauron
Alexander Shulgin Books
We know what they deal with. We didn't just fall off the turnip truck.

Still want to pose like y ...
24-9-2007 at 07:27
by: Sauron
Trialkyl Phosphites from Alkoxide and PBr3?
The situation in USA is going to approach what things were like during WWI when reagent manufacturin ...
24-9-2007 at 05:28
by: Sauron
Cyanide fun question.
Any pesticide industry would have been perverted by Saddam for the purpose of making chemical weapon ...
23-9-2007 at 23:02
by: Sauron
Erratum in Saunders "Phosphorus and Fluorine"
I have not yet obtained the article but no, diethyl hydrogen phosphite is quite stable. See Inorg.Sy ...
23-9-2007 at 18:15
by: Sauron
Trialkyl Phosphites from Alkoxide and PBr3?
I would truly hope that the clueless beginner would have the commonsense to stay away from OP, certa ...
23-9-2007 at 12:40
by: Sauron
Trialkyl Phosphites from Alkoxide and PBr3?
I have nothing truly toxic in mind. The lower trialkyl phosphites are for the final coupling step in ...
23-9-2007 at 12:02
by: Sauron
Trialkyl Phosphites from Alkoxide and PBr3?
I would like to prepare some trialkyl phosphites for various projects. I can't buy these, damn it, n ...
23-9-2007 at 10:58
by: Sauron
Erratum in Saunders "Phosphorus and Fluorine"
I have enough of a headache from the P nomenclature already.

Besides who wants to have to say tet ...
23-9-2007 at 08:37
by: Sauron
Erratum in Saunders "Phosphorus and Fluorine"
While re-reeading B.C.Saunders' excellent little book on organophosphorus and fluorine chemistry, wh ...
23-9-2007 at 07:21
by: Sauron
Red P (higher yeild method)
The matchbook method is not an easy way; it is a time consuming nd laborious way to obtain anything ...
23-9-2007 at 00:14
by: Sauron
chloral hydrate synthesis
Oh, I DO see some rather stupidposts by a guy named punk quite appropriately, BACK ON PAGE 1. THIS I ...
22-9-2007 at 23:13
by: Sauron
chloral hydrate synthesis
What water content?

Ethanol. ANHYDROUS ethanol. Did you bother to read the references?

You wer ...
22-9-2007 at 20:08
by: Sauron
Red P (higher yeild method)
PBr3 like PCl3 reacts vigorously (violently) with water to produce phosphorous acid and HBr. In the ...
22-9-2007 at 20:04
by: Sauron
Red P (higher yeild method)
The last time I got a quote on POBr3 it was a lot costlier than PBr3. That agrees with your own obse ...
22-9-2007 at 10:56
by: Sauron
Red P (higher yeild method)
@woelen, peculiar sounding or not, these are the facts.

I can easily buy PBr3 and have done so, I ...
22-9-2007 at 10:27
by: Sauron
Red P (higher yeild method)
First of all that brand is not sold in this country, it is actually very poorly distributed internat ...
22-9-2007 at 09:41
by: Sauron
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