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Benzodioxole Acetonylation
My point was that they use a whopping excess of aromatic, probably to avoid polycondensation. This i ...
24-2-2012 at 12:58
by: turd
Benzodioxole Acetonylation
If this is the thing Mn(III) thing posted on the rhodium site: Attention, yields are given relative ...
23-2-2012 at 01:19
by: turd
Please welcome our latest moderator, ScienceSquirrel
[rquote=237844&tid=18784&author=AndersHoveland]This [i]is[/i] a science forum. I think we sh ...
22-2-2012 at 04:38
by: turd
Ideas for new hallucinogens?
[rquote=237714&tid=18851&author=GreenD]I laughed when he specifically stated (twice) that he ...
21-2-2012 at 10:48
by: turd
Iodination of p-dimethoxybenzene under non-organic solvent free conditions without organic solvents?
Sure, it's free access, so I hope the authors don't mind.
[file]17627[/file]

Must be a solubilit ...
21-2-2012 at 10:37
by: turd
Iodination of p-dimethoxybenzene under non-organic solvent free conditions without organic solvents?
You are right - the 94% is from Synthesis 2006, 2603–2607.
10 ml H2O per mmol of substrate. That ...
21-2-2012 at 04:41
by: turd
Ideas for new hallucinogens?
[rquote=237634&tid=18851&author=White Yeti]No reason to shun out botany, there are many powe ...
20-2-2012 at 15:31
by: turd
Iodination of p-dimethoxybenzene under non-organic solvent free conditions without organic solvents?
Maybe someone who is smarter than me can explain this:

Acta Chim. Slov. 2008, 55, 841–849
(Fre ...
20-2-2012 at 15:15
by: turd
Ideas for new hallucinogens?
Huh?

The psychedelic effects of 2C-B on normal doses are [i]much[/i] more benign than that of LSD ...
20-2-2012 at 14:57
by: turd
Ideas for new hallucinogens?
[rquote=237429&tid=18851&author=White Yeti]What's the point of synthesising new hallucinogen ...
19-2-2012 at 00:49
by: turd
Epoxidation via peracetic acid
What method are you following or are you improvising??

This here:
http://www.erowid.org/archive/ ...
17-2-2012 at 09:25
by: turd
Epoxidation via peracetic acid
If you want help you will need to describe [i]exactly[/i] what you did. How did you prepare the pera ...
17-2-2012 at 08:58
by: turd
Meta-Escaline via Ullmann on Bourbonal
[rquote=237082&tid=7045&author=DrNoiZeZ]Most of the bromovanillin goes out when you add H20 ...
16-2-2012 at 23:56
by: turd
What to do with tryptamine?
[rquote=236754&tid=18332&author=Bot0nist]So, any luck with that decarboxylation android. Wai ...
16-2-2012 at 02:56
by: turd
Russian HyperLab: reformed and renewed
[rquote=236857&tid=18765&author=entropy51]The present whining is coming from the biggest of ...
16-2-2012 at 02:44
by: turd
Meta-Escaline via Ullmann on Bourbonal
[rquote=236889&tid=7045&author=Scr0t]Yield was 79% of Syringaldehyde after recrystallization ...
16-2-2012 at 02:33
by: turd
Tryptamine refusing to crystallize
[rquote=236694&tid=14147&author=GreenD]I had read somewhere that the bp of tryptamine was 14 ...
13-2-2012 at 11:29
by: turd
Tryptamine refusing to crystallize
First of all, nice to read some real chemistry beyond speculation and crystallization.

But to be ...
13-2-2012 at 00:10
by: turd
Russian HyperLab: reformed and renewed
The quite common (and worthwile!) target DOB has a dose of 2-3 mg. To purify if by distillation with ...
13-2-2012 at 00:04
by: turd
3,4,5-trimethoxy-beta-nitrostyrene synthesis
[rquote=236323&tid=3126&author=mrnye]I found sources for ethylendiamine but they will only s ...
10-2-2012 at 07:25
by: turd
3,4,5-trimethoxy-beta-nitrostyrene synthesis
[quote]EDDA, cyclohexylamine and butylamine aren't commercially available[/quote]
You must be kiddi ...
9-2-2012 at 12:27
by: turd
3,4,5-trimethoxy-beta-nitrostyrene synthesis
What's wrong with EDDA?
[url]https://www.erowid.org/archive/rhodium/chemistry/edda.html[/url]:
[qu ...
9-2-2012 at 00:08
by: turd
Crystal Growing
[rquote=236166&tid=5529&author=GreenD]you guys ever see this cave in russia?

[url]http:// ...
8-2-2012 at 12:38
by: turd
Hate this stuff
There is no point in examples since ALL of chemistry is like that. One reason is that many trivial n ...
7-2-2012 at 11:14
by: turd
Hate this stuff
ITHM that phosgene does not contain phosphorus, chlorophyll no chlorine, chrome alum no aluminium, u ...
7-2-2012 at 08:05
by: turd
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