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Easy-to-synthesize odor compounds
[rquote=669777&tid=158258&author=DraconicAcid]I've had rotten luck with a lot of esters, but ... |
8-1-2022 at 05:37
by: teodor |
The 2021 Christmas greeting thread
For those members who used to celebrate Christmas by the Julian calendar (like me, if any) - Merry C ... |
6-1-2022 at 12:13
by: teodor |
Menthyl acetate
Thanks, mayko.
I will try both methods. Just mixing menthol and acetyl chloride (and allowing HCl ... |
31-12-2021 at 12:14
by: teodor |
Menthyl acetate
I'd like to make this ester of menthol. Could you supply me with the procedure?
It looks like Fisch ... |
31-12-2021 at 09:04
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669123&tid=158187&author=Monoamine]
And by "asleep" you mean forever. Right?  [/ ... |
24-12-2021 at 08:37
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
I am dreaming of getting SOBr2 from the reaction of SOCl2 with BBr3 which is described as good both ... |
24-12-2021 at 04:28
by: teodor |
Synthesis of dichloromethane- question mark.
Chemplayer has a video about the preparation of chloroform from trichloroacetic acid. So, I am wonde ... |
23-12-2021 at 12:37
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
Maybe adducts like Al2Cl6 * SOCl2 could be used to shift an equilibrium during the synthesis. This i ... |
22-12-2021 at 14:51
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669033&tid=158187&author=Bedlasky]
Hi, Teodor. May I ask you where did you read thi ... |
22-12-2021 at 12:55
by: teodor |
Beryllium compounds
"An apparently unique property of beryllium is its tendency to form so-called "basic" derivatives of ... |
22-12-2021 at 08:00
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
Yes, Fery, SOCl2 is nasty, for that reason, I will try the distillation after improving my fume hood ... |
22-12-2021 at 06:14
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
Monoamine,
I have enough quantity of SOCl2 and that is the only reason I don't try to repeat your ... |
21-12-2021 at 07:20
by: teodor |
N2O3 extraction in dichloromethane
The compound NOClO4 is decomposing to a mixture of oxidizers of all kinds: chlorine, oxygen, nitric ... |
21-12-2021 at 04:52
by: teodor |
N2O3 extraction in dichloromethane
It is a very nice experiment and the color of the solution is appealing.
I am thinking about
1 ... |
21-12-2021 at 00:52
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=668852&tid=158187&author=Monoamine]Hi teodor. Do you know how much air (do you mean ... |
20-12-2021 at 14:05
by: teodor |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=668773&tid=158187&author=Monoamine]I now also think I can hazard a guess about my ea ... |
17-12-2021 at 08:13
by: teodor |
Isopropyl Acetate
Interesting. How to lower those byproducts? Does the catalyst (H2SO4/pTsOH/HCl) play a role?
My t ... |
17-12-2021 at 08:00
by: teodor |
Isopropyl Acetate
Hi Fery. I used 0.5 mols of acid per 0.4 mols of alcohol. But with yields > 80% I really don't ne ... |
16-12-2021 at 03:16
by: teodor |
Isopropyl Acetate
By the same method, I've got n-amyl n-butyrate in 82% yield (I measure the yield by the main fractio ... |
15-12-2021 at 13:14
by: teodor |
Locking old threads so people don't reincarnate them.
Probably there are good and bad cases of thread reincarnation. Newton2.0, you said, "I have often ma ... |
14-12-2021 at 08:31
by: teodor |
Toluenesulfonic acid and Sulfonic acids in genera
Now I try to find a way to get anhydrous TsOH from a hydrated form.
Drying in a desiccator (KOH + C ... |
14-12-2021 at 04:33
by: teodor |
Isopropyl Acetate
[rquote=652650&tid=71937&author=Fery]teodor 22 hours for this esterification, wow, so long : ... |
13-12-2021 at 12:17
by: teodor |
Disposal of Nitrogen Oxides
I was thinking about a more stable binding of NO than [Fe(H2O)5(NO)]2+ anion and eventually, I found ... |
12-12-2021 at 08:52
by: teodor |
Toluenesulfonic acid and Sulfonic acids in genera
Could somebody provide the information about the inorganic chemistry of p-toluenesulfonic acid? I kn ... |
11-12-2021 at 06:52
by: teodor |
Chemical demonstration: accurate wind direction detection with tert-butanol
Now I understand why it happens with pure tert-butanol but works neither with glacial acetic acid no ... |
10-12-2021 at 04:02
by: teodor |
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