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Preparation of methyl tosylate, safe methylating agent
HCl shoud be very easy to remove from you final product.
And if you dont want to use tosyl chlori ... |
9-8-2010 at 18:27
by: mnick12 |
The short questions thread (3)
The yield of uncatalized n-propyl formate with 12hrs of reflux is said to be around 65%, so I would ... |
5-8-2010 at 15:20
by: mnick12 |
good pump?
Well I shipped the monster home today, and the beast weighs a littile over 26lbs. It still needs a n ... |
5-8-2010 at 15:14
by: mnick12 |
good pump?
You are right to warn me, and yes I dont much at all about vacuum pumps. That is sort of the reason ... |
2-8-2010 at 15:22
by: mnick12 |
good pump?
So I was looking around in our boat house yesterday, and I found an old vacuum pump. It works fine b ... |
1-8-2010 at 17:26
by: mnick12 |
p-benzoquinone HELP!!!
The way I usually make benzoquinone is from hydroquinone. There are a number of routes out there but ... |
31-7-2010 at 08:12
by: mnick12 |
Making Pentaerythritol in home from easily available chemicals.
You have not shown you have done any work, why should I help you? You could do some research on your ... |
19-7-2010 at 20:15
by: mnick12 |
Informations about nitrosoguanidine?
Here is one from the library
"Preparation of Nitrosoguanidine.25 Twenty-one grams of nitroguanid ... |
19-7-2010 at 12:01
by: mnick12 |
Condenser cooling
Well the peltiers came a few days ago they are neet little things, but I have not had to much time t ... |
16-7-2010 at 23:58
by: mnick12 |
Mom Arrested After Son Makes Dry Ice "Bombs"
This reminds me of that story where a 1st grader (I think dont remember) was suspended for a few day ... |
15-7-2010 at 10:58
by: mnick12 |
ETN Synthesis/Yield Problems
No acetone wont destroy etn, but it will dissolve a large amount of it. When preforming a recrystall ... |
14-7-2010 at 19:01
by: mnick12 |
ETN Synthesis/Yield Problems
How much ETN did you have? 300ml sounds like way to much acetone. Also cooling to rt is not usually ... |
13-7-2010 at 20:37
by: mnick12 |
Synthesis of Solid Calcium Hypochlorite
Well,
You can buy 54% CaOCl at the pool store as pool shock.
I dont think you will have any luck ... |
13-7-2010 at 20:35
by: mnick12 |
Methyl aryl ether demethylation of 4-Allyl-2-methoxyphenol - a LONG discussion
Nice post I enjoy the pics,
I was thinking could aluminum tribromide be used instead? I think it co ... |
13-7-2010 at 09:07
by: mnick12 |
Liquid heat exchangers
Thanks for the ideas.My chips are 40mmX40mm , but they are still in the mail.
I am thinking about ... |
13-7-2010 at 08:53
by: mnick12 |
ETN Synthesis/Yield Problems
Uhhhh thats a little scary, ETN is rather sensitive stuff. Just something to note never use an open ... |
12-7-2010 at 21:36
by: mnick12 |
The Phenacylamines - would Quinacetephenone work?
If you dont want to use nitromethane or nitroethane you could get your amine from an amide or nitril ... |
12-7-2010 at 20:41
by: mnick12 |
ETN Synthesis/Yield Problems
There are already quite a few threads on ETN, use the search engine.
If your having a problem wit ... |
12-7-2010 at 17:32
by: mnick12 |
Oxidation of eugenol to vanillin
Thats interesting, 67% is not great but it is better than I expected for chromic acid. As for anilin ... |
11-7-2010 at 20:58
by: mnick12 |
Novelty explosives
This is not something you really want to make it is really sensitive. But I believe it is called "fu ... |
11-7-2010 at 11:20
by: mnick12 |
RDX E method
Care to provide a reference to what you are talking about? I know of the E method but I am not sure ... |
10-7-2010 at 22:14
by: mnick12 |
Liquid heat exchangers
So I recently ordered some Peltier chips, and as you may know to run properly they need a good way o ... |
10-7-2010 at 17:23
by: mnick12 |
Extracting caffeine from coffee - photo essay
Good job,
I dont know if you have one, but I have heard of caffeine being purified by subliming it ... |
10-7-2010 at 10:28
by: mnick12 |
Oxidation of eugenol to vanillin
Thanks for the tip, I now realize how dangerous microwave reactions can be and have chosen to do a s ... |
10-7-2010 at 10:17
by: mnick12 |
Condenser cooling
I am currently working on a cooler for my condenser that should be able to reach sub-zero temperatur ... |
8-7-2010 at 14:15
by: mnick12 |
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