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Good way to Methylamine HCl?
call me oldschool what's wrong with the traditional way of making methylamines????
if it works why ...
7-7-2009 at 17:53
by: jon
Leuckart reaction

where is that reference that promises 95% yeilds by means of microwave irridatiation???
read it s ...
7-7-2009 at 17:29
by: jon
Chemical clearance NOW ON
i keep hearing about australian customs those guys don't miss a thing do they?
29-5-2009 at 14:24
by: jon
theoretical amphetamine variants
the pharmacuetical companies are always on the hunt for ways to push amphetamine under new patents b ...
29-5-2009 at 13:20
by: jon
Chemicals in Canada
next it will be toilet paper then you won't be able to shit without them knowing how many sheets.
l ...
22-5-2009 at 22:22
by: jon
Caesium (cesium) wanted in the UK
hey hey hey $125/500g (cs2co3) akscientific and tell 'em red sent ya just kiddin
15-4-2009 at 21:37
by: jon
TMA-2: Several questions on a particular synthesis
you're right i can't locate the reference but i know you don't use acids on highly activated rings t ...
25-1-2009 at 10:46
by: jon
Acylation of benzene with anhydrides
polyphosphoric acids are also claimed to work as well.
24-1-2009 at 22:57
by: jon
uc berkerly o-chem on youtube.
watch and learn!
http://www.youtube.com/watch?v=Vv0wVdVd45o
24-1-2009 at 22:11
by: jon
preperation of cumene from isopropanol and benzene
someone on this board at one time was complaining about the difficulty in obtaining p-cumene despite ...
24-1-2009 at 21:38
by: jon
TMA-2: Several questions on a particular synthesis
i have a question about this why not simply halogenate that double propenyl bond then react it with ...
24-1-2009 at 20:55
by: jon
Willgerodt Reaction
theres also the sodium dichromate oxidation of m-amino-1-ethylbenzene as a possibility.
13-1-2009 at 11:51
by: jon
Willgerodt Reaction
what about the grignard intermediate react with co2 and quench thought about that?
example:
m-ami ...
12-1-2009 at 23:11
by: jon
Morpholine derivate from secondary amine/alcohol
right, that's what he's driving at, 2-iodoethanol, k2co3, ephedrine, and methanol reflux it.
but wh ...
12-1-2009 at 22:25
by: jon
prepn. of anhydrous hbr with NaHSO4 and NaBr
not to mention the stench i would'nt even think it would stay in solution
28-12-2008 at 18:38
by: jon
prepn. of anhydrous hbr with NaHSO4 and NaBr
it works with table salt to make dry hcl gas, i'll have to find out for myself i remember though it ...
27-12-2008 at 22:18
by: jon
Drying HBr... has anyone considered this?
well instead of starting a new thread i should have done this.
what about heating NaHSO4 with NaBr? ...
27-12-2008 at 20:47
by: jon
prepn. of anhydrous hbr with NaHSO4 and NaBr
has anyone considered this?
you know the sulfate anion oxidizes hydrogen bromide but as a dry mixtu ...
27-12-2008 at 20:30
by: jon
direct hydroamination of olefins with biscyclopentadiene samarium complex catalysis
well to say the least distlilling over na/k three times is tedious having to do everthing in an iner ...
15-12-2008 at 18:23
by: jon
direct hydroamination of olefins with biscyclopentadiene samarium complex catalysis
yeah you're sure right about that the solvents have to be degassed to avoid poisoning the catalyst, ...
15-12-2008 at 07:32
by: jon
direct hydroamination of olefins with biscyclopentadiene samarium complex catalysis
you guys especially you bees out there might be interested in the possibilty of adding primary amine ...
14-12-2008 at 18:40
by: jon
Drying HBr... has anyone considered this?
that was exactly what i read on a page from a chinesse supplier ( about the clumping)the easiest way ...
3-11-2008 at 17:45
by: jon
Drying HBr... has anyone considered this?
right it's got to be concentrated and above a certain temperature 60 C I think for that to happen.
...
3-11-2008 at 13:13
by: jon
Drying HBr... has anyone considered this?
as was stated before it takes a tremendous amount of heat to get that to work you'll likely eat the ...
2-11-2008 at 21:50
by: jon
Drying HBr... has anyone considered this?
i saw the one on orgsyn and oh what a pain! why do people go through the elbows to get to the asshol ...
2-11-2008 at 21:21
by: jon
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