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Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
@ tentacles

I did my dissolution in a 100 or 150 ml beaker, about half full of 68% nitric acid, s ...
13-2-2008 at 17:04
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
@ Rosco, tentacles

Yeah, there is no problem with wetability. I didn't worry about the filtering ...
13-2-2008 at 10:34
by: Xenoid
Oxidative Soak
[color=red]@Rosco - this is for you![/color]

I've just started another anode, this one is destine ...
12-2-2008 at 20:42
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
@ Rosco

We still seem to be running around in circles, [color=red]it would be really nice if some ...
12-2-2008 at 01:09
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by dann2[/i]
Have you tried running the Mn Oxide anode in a Perchlorate ...
11-2-2008 at 19:28
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by tentacles[/i]
I wonder what would happen if the oxidative soak was t ...
10-2-2008 at 11:41
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by tentacles[/i]
Haven't been messing with anodes for the last week, I' ...
10-2-2008 at 09:43
by: Xenoid
PC PSU to laboratory PSU
@ Der Alte

Clearly you are not reading my posts correctly .... :mad:

NOWHERE have I claimed th ...
2-2-2008 at 23:38
by: Xenoid
PC PSU to laboratory PSU
@ Dann2

Well there are perchlorate cells and perchlorate cells, mine have operated in the 4 - 4.5 ...
2-2-2008 at 20:35
by: Xenoid
Platinum plated titanium
@ markgollum

At this stage I think it is a matter of "suck it and see". I don't think you will fi ...
2-2-2008 at 19:23
by: Xenoid
No User Serviceable Components Inside
Here is the ATX PSU I have modified with current control, using the simple circuit from the site ori ...
1-2-2008 at 17:33
by: Xenoid
The lead salts preparation thread!
[quote][i]Originally posted by Xenoid[/i]

Lead nitrate IS white, it's not colourless. White cryst ...
28-1-2008 at 17:54
by: Xenoid
Lithium (Per)Chlorate cell
Well I think that is very high!

I don't even run Pt that high, but I'm pretty conservative on thi ...
28-1-2008 at 14:00
by: Xenoid
Lithium (Per)Chlorate cell
@ hashashan

Are you putting to much current through your cell, what current density are you runni ...
28-1-2008 at 13:27
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by chloric1[/i]
..... I don't know how I missed that reference. [/quote ...
27-1-2008 at 18:20
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
@ chloric1

Details please! Did you dip and shake, dry at low temperature, use an alcohol in your ...
27-1-2008 at 15:42
by: Xenoid
Hubert Update
Hubert and "Purple Haze" are still running well and producing KClO3 for me. Hubert has been running ...
26-1-2008 at 22:44
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by dann2[/i]
...... It will make mass production a reality............. ...
26-1-2008 at 19:06
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by tentacles[/i]
.... then add a splash of H2O2, the whole solution foa ...
26-1-2008 at 15:27
by: Xenoid
The lead salts preparation thread!
@ chloric1

Actually the solution was not really "dirty green". I only filtered the solution using ...
25-1-2008 at 20:08
by: Xenoid
The lead salts preparation thread!
[quote][i]Originally posted by Aqua_Fortis_100%[/i]

Why dont use this?
Assuming that in some pla ...
25-1-2008 at 16:22
by: Xenoid
Lead Nitrate
Lead nitrate is the most soluble lead salt (55g/100g water), and is a popular choice for a plating b ...
25-1-2008 at 12:07
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
@ chloric1

That looks pretty damn hot in there ... :o

How are you mounting the rod(s) with a h ...
24-1-2008 at 16:37
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Well, my antimony, tin and bismuth finally arrived today. They were rattling around in the bottom of ...
22-1-2008 at 16:24
by: Xenoid
Lithium (Per)Chlorate cell
Yes, I suppose in retrospect it was! Really, I was just trying out the procedure!

My Li2CO3 was a ...
21-1-2008 at 10:28
by: Xenoid
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