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CS2 a Different Way
Make up whatM Garlic suggested allyl sulfide to me, further reading revealed the culprit to be thiop ...
22-5-2009 at 03:26
by: Sauron
CS2 a Different Way
The thiophenol need only be present in very low concentration to impart that odor. It's obnoxious st ...
22-5-2009 at 02:12
by: Sauron
CS2 a Different Way
Well, acetylene is readily available at any welding supply shop in various sizes of cylinder, and re ...
22-5-2009 at 01:20
by: Sauron
CS2 a Different Way
Yes, g c, precisely why I thought it noteworthy. Most likely my equation is inaccurate, but, maybe n ...
21-5-2009 at 21:37
by: Sauron
CS2 a Different Way
Thanks, S.C.

Here is the J.Chem.Soc. paper. The reaction does work, optimally at c.500 C and abou ...
21-5-2009 at 19:51
by: Sauron
CS2 a Different Way
According to Mellor. passing acetylene into molten sulfur produces CS2. I have yet to try to dig out ...
21-5-2009 at 11:48
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Hector, clumsy attempts at deceiving this forum do you no credit.

I am afraid you have mplaced yo ...
17-5-2009 at 22:23
by: Sauron
The WORST BOOKS Ever Written
Read the thread and you will be forced to come to the unalterable conclusion that this is anything b ...
17-5-2009 at 04:00
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
OK hector, do what you want.

You will find the resolution of PAC tedious and expensive I think. A ...
17-5-2009 at 03:34
by: Sauron
The WORST BOOKS Ever Written
"Angels and Demons"

for wholesale anachronism and buthery of history

Ha;i;eo died 200 years be ...
16-5-2009 at 22:22
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Hector, tartaric acid is simply an example.

It may or may not be effective for the resolution of ...
16-5-2009 at 22:04
by: Sauron
How many indole alkaloids in natural products?
How many indole angels can dance on the head of a pin?

The question can be answered obly by usin ...
14-5-2009 at 06:15
by: Sauron
KINDLY STAY ON TOPIC!
Learn some stereochemistry and the answer will pop out.

Your question is a good one. HOWEVER, thi ...
13-5-2009 at 11:57
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Hector

Follow thw protocol in JACS

If it says mandelamine hcl, use that

Otherwise use free ...
12-5-2009 at 01:27
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Bandying words with turd is not a productive pasttime. He's out to wreck this thread, not to enlight ...
11-5-2009 at 19:01
by: Sauron
Anyone have Practical Experience with Polymer Synthesis?
Thanks!
11-5-2009 at 05:54
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Here is the Org.Syn. prep of MeI by two methods.

Others give you citations, I give you PDFs.
11-5-2009 at 05:32
by: Sauron
Stability of cyanuric chloride at room temperature?
The short answer is No,

Don't heat it to decomposition.

Read Ullmann.
11-5-2009 at 00:56
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Hector

The cost of MeI is of no concern if you simply make your own.

Two methods are detailed ...
11-5-2009 at 00:14
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Hector

To make L-PAC you must use d-mandelic acid to make d-mandelamide.

This is by definition ...
10-5-2009 at 09:39
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
Recommending ;ithiarion to someone who ubtil a week or 10 days ago had never done a Grignard strikes ...
10-5-2009 at 05:39
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
L-PAC is not a controlled substance, and anyway the forum policy is to be unconcerned with law is it ...
9-5-2009 at 19:17
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
I see. Well as far as I recall hector has only asked about acetic anhydride, which many of us want, ...
9-5-2009 at 19:00
by: Sauron
Synthesis of L-Phenylacetylcarbinol(L-PAC)
First of all, I am only interested in the chemistry and not at all in making PAC, ephedrine or anyth ...
9-5-2009 at 17:53
by: Sauron
Stability of cyanuric chloride at room temperature?
Oh, it's useful stuff, particularly for alkyl chlorides and bromides, and acyl chlorides.

The on ...
9-5-2009 at 16:54
by: Sauron
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