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Ester to Acid Chloride in One Step
Phthaloyl chloride is not too hard to make, benzotrichloride and phthalic anhydride in an autoclave ... |
2-10-2007 at 21:26
by: Sauron |
P4O10 and P4S10 w/Oxalyl Chloride
Some basics
Hydrolysis of P4S10
This is instructive because it is the simplest case of the thi ... |
2-10-2007 at 19:25
by: Sauron |
Effect of leaving group on organophosphate toxicity
Succinylcholine acts as a depolarizing neuromuscular blocker. It imitates the action of acetylcholin ... |
2-10-2007 at 17:37
by: Sauron |
Reduction Al-Hg
@Nicodem, this thread has no raison d'etre at all, other than to assist filemon with his reduction ... |
2-10-2007 at 16:46
by: Sauron |
Effect of leaving group on organophosphate toxicity
There were, or so I am told, low level exosures of troops that occurred due to strikes on some of Sa ... |
2-10-2007 at 10:11
by: Sauron |
Ester to Acid Chloride in One Step
The combination of phthaloyl chloride and chlorosulfonic acid has been found to directly convery car ... |
2-10-2007 at 07:12
by: Sauron |
Reduction Al-Hg
True but a little less than germaine. The chap's reaction did not work, despite all of that. So why ... |
2-10-2007 at 06:18
by: Sauron |
P4O10 and P4S10 w/Oxalyl Chloride
Back to P4S10 electrophilic substitution reaction with anisole.
It seems that the 24 hr reaction ... |
2-10-2007 at 00:52
by: Sauron |
Reduction Al-Hg
I don't care if some one wants to make MeNH2.
And I also don't care if someone wants to make a CW ... |
1-10-2007 at 21:46
by: Sauron |
Reduction Al-Hg
He was using neither HCl not EtOH. He was using AcOH, go read his post.
And he gpt no reduction.
... |
1-10-2007 at 21:42
by: Sauron |
Effect of leaving group on organophosphate toxicity
There's more than one sort of human AChE
And more than one mode of action.
More than one aspe ... |
1-10-2007 at 18:49
by: Sauron |
Reduction Al-Hg
I was going to suggest Fe or Sn either one with HCl, classic dissolving metal reduction.
I think ... |
1-10-2007 at 10:42
by: Sauron |
Thionyl chloride and acetone, what happens?
About the only thing that popped out of that reference was a compound I first encountered a few days ... |
1-10-2007 at 10:11
by: Sauron |
Reduction Al-Hg
Surely there's an embarassment of choices of reducing agents for that one? |
1-10-2007 at 10:02
by: Sauron |
Phenyldichlorophosphine, Useful Reagent
The literature has confirmed that dialkyl alkylphosphonates are cleaved to the corresponding dichlor ... |
1-10-2007 at 09:58
by: Sauron |
Chemistry equipment
Grahan condensers are for vacuum distillations, they serve to increase the dwell time of the vapo in ... |
1-10-2007 at 02:09
by: Sauron |
Phenyldichlorophosphine, Useful Reagent
The reaction of alkyl halides with PCl3 and AlCl3 to form alkylphosphic acids, alkylphosphonyl dichl ... |
30-9-2007 at 22:08
by: Sauron |
Reduction Al-Hg
You want to reduce AcOH?
The active reducing agent in an Al amalgam reduction is the aluminum alk ... |
30-9-2007 at 20:40
by: Sauron |
P4O10 and P4S10 w/Oxalyl Chloride
Traditionally the routes into the R-phosphonic acids
R-P(O)(OH)2
have been few. In the late 19 ... |
30-9-2007 at 19:40
by: Sauron |
Effect of leaving group on organophosphate toxicity
Not to worry.
When I first joined I posted about some of these, but since then I have realized (a ... |
30-9-2007 at 06:39
by: Sauron |
Effect of leaving group on organophosphate toxicity
You are talking about first generation chemical weapons.
1) The forum proprietor prefers that thi ... |
29-9-2007 at 21:24
by: Sauron |
hacked
Why don't you post this warning in same thread as the troublesome post, and contact JohnWW and ask h ... |
29-9-2007 at 14:50
by: Sauron |
P4O10 + alcohol ---> ?
Suffice it to say that P4O10 is an incompatible dessicant for alcohols, amines, phenols etc. Also am ... |
29-9-2007 at 14:43
by: Sauron |
P4O10 and P4S10 w/Oxalyl Chloride
The reaction of P4O10 wurh benzene under autogenous pressure in an autoclave (275 C, 24 hrs) is inte ... |
29-9-2007 at 14:15
by: Sauron |
P4O10 and P4S10 w/Oxalyl Chloride
Not to worry.
Gmelin is not a book but a massive mult-shelf collection of books, so good luck on ... |
29-9-2007 at 03:51
by: Sauron |
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