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mystery reaction...?
Aluminum and not just foil, dissolves in bases. Sodium carbonate being a salt of a very weak acid is ... |
6-10-2007 at 21:45
by: Sauron |
Bromine Source and Synthesis
If I did the sums right, a Kg of the hydantoin is about 4 moles. So you ought to get 2 mols of Br2 ( ... |
6-10-2007 at 20:35
by: Sauron |
pilot plant production of HCN
HCN explosively pooymerizes to cyanuric acid.
JohnWW, if you are skeptical about such polymerizat ... |
6-10-2007 at 19:55
by: Sauron |
Glassware in Texas - Register or Not?
Magic, you pulled a single paragraph totally out of contest from the Arkansas State Plant Board's we ... |
6-10-2007 at 10:44
by: Sauron |
pilot plant production of HCN
This sounds like a recipe for disaster. The only thing worse than HCN is hot angry HCN. HCN loves to ... |
6-10-2007 at 08:47
by: Sauron |
recorder pens
I take it that P-E is no help?
Most likely there is some aftermarket company that does nothing bu ... |
5-10-2007 at 22:09
by: Sauron |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
Chem. Berichte prior to 1902 is available free from Gallica but you have to download page by page.
... |
5-10-2007 at 15:52
by: Sauron |
DIY hydrogenator...
JCE (Journal of Chemical Education) had a peper on the construction of a containment for a Parr or e ... |
5-10-2007 at 06:46
by: Sauron |
adapting a domestic MW
Did anyone find the article I referred to in one of the earliest posts?
A lot of this talk is ans ... |
4-10-2007 at 21:20
by: Sauron |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
And here is the Ber. paper from 1908.
My German is none too perfect so I could have missed someth ... |
4-10-2007 at 16:02
by: Sauron |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
Agreed. I did pull up the very first prep of oxalyl chloride, from diethyl oxalate and PCl5. No equa ... |
4-10-2007 at 07:40
by: Sauron |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
It's unimportable here. Defense Ministry regs.
And I'm going by the equation in Sartori, see the ... |
4-10-2007 at 06:47
by: Sauron |
Effect of leaving group on organophosphate toxicity
No problem.
Glad to clarify. |
3-10-2007 at 23:00
by: Sauron |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
Clearly, what I said was that the reaction of PCl5 and oxalic acid (anhydrous) does not generate any ... |
3-10-2007 at 19:55
by: Sauron |
Glassware in Texas - Register or Not?
Rosco says take the advise of his lawyer friend. I say the lawyers are to blame, the Bard was right, ... |
3-10-2007 at 18:30
by: Sauron |
Reduction Al-Hg
@Sergei, what I object to is Nicodem's unwillingness to help the thread author.
@Filemon, why do ... |
3-10-2007 at 18:19
by: Sauron |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
(COOH)2 + PCl5 -> (COCl)2 + POCl3 + H20
Neither HCl nor CO2 is evolved in that reaction. But t ... |
3-10-2007 at 07:45
by: Sauron |
HOOC-COOH + SOCl2 -> ClOC-COCl ?
This reaction is done neat, in absence of solvent.
Here's Sartori:
Much better than the garble ... |
3-10-2007 at 06:59
by: Sauron |
Phenyldichlorophosphine, Useful Reagent
The full title of the journal is
Berichte der Bunsengesellschaft, Physik Chemie
I have been un ... |
3-10-2007 at 06:16
by: Sauron |
Glassware in Texas - Register or Not?
There are NO laws that restrict how an individual may make use of a product he purchases, with a few ... |
3-10-2007 at 04:20
by: Sauron |
P4O10 and P4S10 w/Oxalyl Chloride
As the attached paper demonstrates, the crude neutral fraction of the reaction product of alcoholysi ... |
3-10-2007 at 02:04
by: Sauron |
Thionyl chloride and acetone, what happens?
So PCl5 does this sometimes, maybe.
There are some caveats. Aryl ketones give a-chloroolefins. No ... |
3-10-2007 at 01:03
by: Sauron |
Phenyldichlorophosphine, Useful Reagent
AlCl3-POCl3 complex is a granular solid that is filtered off from the reaction mixture(s).
I woul ... |
3-10-2007 at 00:58
by: Sauron |
Glassware in Texas - Register or Not?
@pantone, let me rearrange that list to group the chemicals together by product they are precursors ... |
2-10-2007 at 21:56
by: Sauron |
Glassware in Texas - Register or Not?
I see it's a safe bet you never went to law school.
Those are not LAWS.
And they have approxim ... |
2-10-2007 at 21:53
by: Sauron |
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