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Piracetam from 2-Pyrrolidone
I think these guys are joking or being sarcastic.
15-10-2007 at 08:34
by: Sauron
Piracetam from 2-Pyrrolidone
Well, I'm a sissy then. There are worse things than lacrimators. I'm an old chemist, not a bold one ...
14-10-2007 at 15:21
by: Sauron
Piracetam from 2-Pyrrolidone
With a hood, not a big problem.

Use goggles and gloves and keep the sash down as much as possible ...
14-10-2007 at 08:18
by: Sauron
Methylamine Purification
Dimethylamine is employed in the making of GA tabun nerve agent.

So the governments are a wee bi ...
14-10-2007 at 07:05
by: Sauron
Piracetam from 2-Pyrrolidone
Indeed, in Example 1 and some of the subserquent examples in the US patent cited by the thread autho ...
14-10-2007 at 04:12
by: Sauron
Oxidation of THF with nitric acid
4-aminobutyraldehyde diethylacetal is $4 per gram in 100 g packing, and that would be $8 a gram by t ...
14-10-2007 at 00:34
by: Sauron
Piracetam from 2-Pyrrolidone
The example I am sending him to in OS is as stated, he can sort out how to use ethyl bromoacetate in ...
13-10-2007 at 22:50
by: Sauron
Piracetam from 2-Pyrrolidone
That's the way to do it if you can't find the complete prep in the literature.

Searching the lite ...
13-10-2007 at 21:14
by: Sauron
Oxidation of THF with nitric acid
I have stumbled across a use for 4-aminobutyraldehyde diethylacetal and the stuff is commercial but ...
13-10-2007 at 15:13
by: Sauron
Reduction of Aromatic Nitro compounds with Zn / HCl A write up
Good point. It was the thread author who seems fixated on dissolving metal reductions. You are quite ...
13-10-2007 at 04:43
by: Sauron
Reduction of Aromatic Nitro compounds with Zn / HCl A write up
So separate the nitrotoluene isomers and reduce the o-toluene.

And use Sn not Zn.
13-10-2007 at 03:49
by: Sauron
HCN produced using an arc?
DILUTE mineral acid.

Potassium ferrocyanide is easier to buy, and used to be the main bench scale ...
12-10-2007 at 21:48
by: Sauron
3 dimethylamino indole ?
brother Nicodem, this young man would not gave gotten very far if he UTFSE for 3-dimethylaminoindole ...
12-10-2007 at 01:10
by: Sauron
3 dimethylamino indole ?
BTW indole-3-acetic acid is easily made in an autoclave (pressure reactor) from indole, aqueous glyc ...
11-10-2007 at 23:55
by: Sauron
3 dimethylamino indole ?
Nope

If that's what the "text" says then the text is not worth the paper it is written on.

Let ...
11-10-2007 at 21:37
by: Sauron
Glassware in Texas - Register or Not?
Making your own glassware would still mean importing blank glassmaker's supplies and ground glass jo ...
11-10-2007 at 20:56
by: Sauron
HCN produced using an arc?
Try reading Ullmann's and Kirk-Othmer's as recommended in the forum FAQ. They detail industrial proc ...
11-10-2007 at 20:50
by: Sauron
We're back
I can tell you that running up a high post count appears to inspire resentment (jealousy?) and gets ...
11-10-2007 at 20:45
by: Sauron
3 dimethylamino indole ?
DMT is not 3-dimethylaminoindole. It is Dimethylaminoethylindole.

Tryptamine is 3-(2-aminoethyl) ...
11-10-2007 at 20:28
by: Sauron
We're back
Or dispense with the post counter and ranking altogether, if it is troublesome in cases like this, a ...
11-10-2007 at 20:03
by: Sauron
We're back
Polverone makes a very strong case for there being no hack involved. Under the circumstances I think ...
11-10-2007 at 19:44
by: Sauron
We're back
I do not believe that Polverone's editing brought about the outage. I believe a hack did occur, whil ...
11-10-2007 at 18:44
by: Sauron
iodation of double bond benzalacetone
Hmmm, you mean addition to PhCH=CH-C(=O)-Me?

A tug of war between the benzylic H and the alpha-ca ...
11-10-2007 at 17:24
by: Sauron
What are these compounds called?
IIRC quadricyclane was described as an experimental aerospace fuel.

It is valence isomer of bicyc ...
10-10-2007 at 05:52
by: Sauron
phosphorus oxychloride (POCl3)
It's a forum. All members are free to post in any thread. It's not "your" thread. It's Polverone's t ...
10-10-2007 at 05:31
by: Sauron
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