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Dimethylaminoethanol chlorination
You can use chloroacetyl chloride instead to get indol-3-yl chloromethyl ketone, alkylate your amine ... |
19-4-2008 at 06:12
by: Nicodem |
Organoboron enolization reagent for a tertiary amide
I don't think Et3N is basic enough to appreciably promote the enolization of the imide. I think it i ... |
19-4-2008 at 04:39
by: Nicodem |
Finally! Povidone iodine extraction (this one works way better than Rhodiums extraction method)
[quote][i]Originally posted by LSD25[/i]
Wouldn't the PVP-I2 complex bear some resemblance to somet ... |
19-4-2008 at 02:47
by: Nicodem |
pinacol rearragement
I don't think you can get a pinacol-pinacolone rearrangement on such a glycol. Generally only tetras ... |
19-4-2008 at 02:01
by: Nicodem |
Finally! Povidone iodine extraction (this one works way better than Rhodiums extraction method)
[quote][i]Originally posted by LSD25[/i]
Iodine: http://en.wikipedia.org/wiki/Iodine - BP 184.3C
... |
19-4-2008 at 01:08
by: Nicodem |
Separation of Copper/Nickel Alloy
This topic of Cu&Ni salts separation was already discussed in another thread. At that time I pro ... |
19-4-2008 at 00:49
by: Nicodem |
strontium aluminate
What kind of homogenization did you use? Have you tried a planetary mill or just the classical morta ... |
17-4-2008 at 10:56
by: Nicodem |
Dimethylaminoethanol chlorination
It is interesting that though the MSDS of this compound's hydrochloride does not mentions any carcin ... |
17-4-2008 at 10:20
by: Nicodem |
Dimethylaminoethanol chlorination
Well, yes, more than saying this compound [i]is[/i] nitrogen mustard, I was more like warning that i ... |
17-4-2008 at 08:46
by: Nicodem |
Dimethylaminoethanol chlorination
2-Chloroethyldimethylamine is a nitrogen mustard type of compound so don't go easy on it. Its hydroc ... |
17-4-2008 at 05:42
by: Nicodem |
Decarboxylation with H2SO4?
You should explain what you mean. What type of decarboxylation and what type of substrate and so on? ... |
17-4-2008 at 05:34
by: Nicodem |
In Search of NaBH4
GC, yes, I remember you once explained about those regulations in Germany. Quite unfortunate given t ... |
15-4-2008 at 05:57
by: Nicodem |
In Search of NaBH4
Just think about it for a minute.
Why would someone want to go as far as searching for a contact ... |
15-4-2008 at 04:59
by: Nicodem |
In Search of NaBH4
There is no popular illegal drug cooking method that strictly requires NaBH4 and has no alternative. ... |
15-4-2008 at 03:16
by: Nicodem |
6-hydroxy-2-nitrobenzaldehyde
I think the major product is the desired 6-hydroxy-2-nitrobenzaldehyde since in one of the abstracts ... |
14-4-2008 at 12:21
by: Nicodem |
6-hydroxy-2-nitrobenzaldehyde
Well, if you take m-nitroaniline as the starting point, then it is actually economic. You can find t ... |
14-4-2008 at 09:43
by: Nicodem |
thf oxidation
I don't know if it is possible, but the last time it was discussed I could provide no one step metho ... |
14-4-2008 at 08:53
by: Nicodem |
thf oxidation
That paper is quite interesting as it describes a simple method for synthesis of bromohydrines witho ... |
14-4-2008 at 07:32
by: Nicodem |
worst stench
[quote][i]Originally posted by DNA[/i]
Lately I smelled benzylmercaptan or better known as the abov ... |
14-4-2008 at 04:36
by: Nicodem |
Where, or how can i get Alagebrium?
Thiazole and Its Derivatives was already scanned. I uploaded it in References right now. |
13-4-2008 at 23:51
by: Nicodem |
6-hydroxy-2-nitrobenzaldehyde
Stoichiometric_steve, reduction of m-dinitrobenzene to m-nitroaniline can be performed selectively w ... |
13-4-2008 at 23:28
by: Nicodem |
Organoboron enolization reagent for a tertiary amide
Dibutylboron trifluoromethanesulfonate is commercially available a Acr*s.
You can use LDA in THF (k ... |
11-4-2008 at 22:57
by: Nicodem |
Fresh Look at Sulfur Halide Rxn w/Acyl Salts
[quote][i]Originally posted by len1[/i]
The similarity is in the starting materials and the product ... |
10-4-2008 at 07:55
by: Nicodem |
aldehydes and ketones by dry distillation: practical details?
I thought it was me who invented that phrase. 
Indeed in the literature it is most commonly refer ... |
10-4-2008 at 03:39
by: Nicodem |
Fresh Look at Sulfur Halide Rxn w/Acyl Salts
[quote][i]Originally posted by len1[/i]
I am very surprised by this method. It is essentially iden ... |
9-4-2008 at 23:26
by: Nicodem |
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