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What is this sludge in my perchlorate cell?
Then if current went low you probably don't have your buss bars or contacts copper plated

PbO2 do ...
7-12-2020 at 00:12
by: mysteriusbhoice
What is this sludge in my perchlorate cell?
best to specify what electrodes he is using because at this point it just looks like a chlorate cell ...
6-12-2020 at 19:29
by: mysteriusbhoice
Electrosynthesis of nitrates from urine
som1 told me to try using cyanuric acid instead of urea for anodic oxidation
https://www.sciencemad ...
6-12-2020 at 10:33
by: mysteriusbhoice
More on PbO2 electrodes
one of my latest runs with it


[file]85063[/file] [file]85065[/file] [file]85067[/file]

old ...
6-12-2020 at 10:25
by: mysteriusbhoice
What is this sludge in my perchlorate cell?
iron can kill some MMO btw if thats what you were using to convert NaCl into chlorate.
Shoulda adde ...
6-12-2020 at 10:22
by: mysteriusbhoice
How to build a cheap and durable electrolytic cell
10 USD uhhh well just get a plastic bottle or a mug and a popsicle stick and drill 2 holes and for p ...
3-12-2020 at 01:22
by: mysteriusbhoice
perchlorate cell questions
when does ozone evolution take place in the cell and does that affect PbO2 in terms of wear rate.
2 ...
3-12-2020 at 00:20
by: mysteriusbhoice
More on PbO2 electrodes
this electrode is amazing!!!
legit its running its 2nd batch now and holding strong this time.
lea ...
2-12-2020 at 05:35
by: mysteriusbhoice
Electrosynthesis of nitrates from urine
You need sodium perchlorate catalyst for this process and also membrane cell and PbO2 electrode memb ...
1-12-2020 at 20:59
by: mysteriusbhoice
perchlorate cell questions
Anyways it turns out my homemade PbO2 electrode from lead chlorate works really well and I'm current ...
1-12-2020 at 20:42
by: mysteriusbhoice
perchlorate cell questions
finally producing product video of cleanup soon!!
28-11-2020 at 03:56
by: mysteriusbhoice
perchlorate cell questions
so I ran my perchlorate cell for 1 day at 14 amps 180ma/cm^2 with my MMO PbO2 plate anode and Ti mes ...
27-11-2020 at 05:29
by: mysteriusbhoice
More on PbO2 electrodes
made another one of these this time plated with ultrasound and very low current density of 6ma/cm^2
...
17-11-2020 at 12:05
by: mysteriusbhoice
Lead Ion perchlorate cell test.
yea cell is usually covered with super absorbant cloth while running and btw rn im plating MMO with ...
17-11-2020 at 03:21
by: mysteriusbhoice
Restoration of MMO electrode using lead chlorate PbO2 bath
I had a slightly damaged MMO anode from salt cake electrolysis to produce HCl via membrane from my p ...
14-11-2020 at 12:51
by: mysteriusbhoice
More on PbO2 electrodes
so I first plated PbO2 onto EDM graphite and got a uniform coating that had lots of pits due to this ...
12-11-2020 at 13:20
by: mysteriusbhoice
Lead Ion perchlorate cell test.
this time coated EDM graphite and ended up with this
vid below:
https://youtu.be/bukb01EiY0k
10-11-2020 at 00:26
by: mysteriusbhoice
Lead Ion perchlorate cell test.
so uhh ive ran my lead ion perchlorate cell and made a friggin GSLD that was made in lead perchlorat ...
9-11-2020 at 13:45
by: mysteriusbhoice
More on PbO2 electrodes
I have also included a pic of my lead ion perchlorate cell here with the lead ion feeder to buildup ...
6-11-2020 at 04:53
by: mysteriusbhoice
Lead Ion perchlorate cell test.
I can even add a lead electrode + resistor or sth to act as a 2nd anode which will keep lead ions in ...
6-11-2020 at 04:03
by: mysteriusbhoice
Lead Ion perchlorate cell test.
I recently thought of a new idea and thats with regards to the stability of perchloric acid which me ...
6-11-2020 at 03:48
by: mysteriusbhoice
Perchlorate cell additives for Pt anode
[rquote=647676&tid=155572&author=Antiswat]so, mysteroisbchoice, 1.4kg in 4 days? how many am ...
29-10-2020 at 21:41
by: mysteriusbhoice
Compact Flow-Through Electrochemical Cell for Perchlorates
MMO wont erode in a perchlorate cell if its only used as a carrier and not the main electrode but I ...
5-10-2020 at 22:35
by: mysteriusbhoice
Single component rocket fuels
[rquote=645789&tid=156258&author=aromaticfanatic]I've quit explosives for a while now but my ...
5-10-2020 at 01:34
by: mysteriusbhoice
A slightly dangerous but surprisingly effective way to make HCl
the HCl generator is finalized using the new 4 liter MMO salt cake PVA ion exchange membrane cell an ...
3-10-2020 at 03:22
by: mysteriusbhoice
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