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Diethyl amine turning brown
it happened to me well not exactly but handling so much methylamine i finally got a compliant i poin ...
25-6-2010 at 13:43
by: jon
Diethyl amine turning brown
your neighbors may think your running whore house, careful!!!
25-6-2010 at 06:47
by: jon
Acetaldehyde synthesis
cyanide became safe to handle??
did i just read that????
or am i on drugs?
23-6-2010 at 22:16
by: jon
debrominating 2-Br-Lysergic Acid / Lysergamides
would this approach be less likely to cause aromatic irreversable isomerization??

pp 616-618

h ...
23-6-2010 at 21:23
by: jon
tetra butyl ammonium bromide
I swear nicodem are you sure you did'nt co-author "advanced organic chemistry" j. march. ???
I ask ...
2-4-2010 at 05:41
by: jon
Bad days in the lab or with glassware?
this one was bad a heavy walled flask used for a pressure rxn unbeknownst to me had a star crack.
...
1-4-2010 at 05:43
by: jon
vacuum distillation
in the above case sometimes inert gasses are used to prevent oxidation, higher boiling inert miscibl ...
1-4-2010 at 04:43
by: jon
Amino alcohol via Akabori, trial run
u know there have been longwinded arguments about oxazolidones and such on other forums ,and america ...
8-12-2009 at 16:57
by: jon
Зaйцев's rule
this is thermodymnamic rxn control. you can conrol rates w/ temp. and concentration. kinetic contro ...
16-11-2009 at 20:45
by: jon
4-alkylthio-2,5-dimethoxybenzaldehyde, Sulfuric Duff reaction
what a badass!!! ;)
mr ulmann love your intellect can we switch brains?
i'll be glad to trade you!
13-11-2009 at 05:27
by: jon
Interesting uses of caffein?
viagra starts w caffiene
10-11-2009 at 20:53
by: jon
Hydriodic reducing power
hi will not reduce terminal iodoalkanes except very slugglishly like a week or mor so yes it would w ...
9-11-2009 at 16:17
by: jon
Amino alcohol via Akabori, trial run
they are using 1/1 stochiometry there that's why geez i'm retarded and i can figure that, out unlike ...
9-11-2009 at 16:11
by: jon
Reductive amination and water
A good compound to remove water from the reaction as it is formed from the reaction (MgSO4 ex.)


...
9-11-2009 at 15:42
by: jon
Preventing light from screwing with an electrophilic addition reaction
it's not that touchy keep it on the freeze sealed up it's dark in the freezer.
the cooler the bette ...
9-11-2009 at 15:39
by: jon
propionic anhydride
it works for sure done it myself even penned that quote
9-11-2009 at 15:36
by: jon
"Requests" Eschweiler-Clarke reaction
1 liter of amine methylation wit some of dat formic acid and that formaldehyde oh yeah got the schem ...
9-11-2009 at 15:35
by: jon
Preparation of methyl tosylate, safe methylating agent
nabh4 and formalin read up
14-10-2009 at 22:38
by: jon
cinnamic acid
that's a tough mechanism to pick apart.
5-9-2009 at 14:15
by: jon
cinnamic acid
hmm jon is interested in cinnamic acid esters also cinnamic anhydride is easily prepared from this ...
4-9-2009 at 13:57
by: jon
Monomethylation of primary amines: N-methyl-2-phenethylamine
perhaps you are right but formaldimes are pretty stable entities and they tend to form at wider ph r ...
3-9-2009 at 22:30
by: jon
1-bromo-3,4-methylenedioxybenzene uses
mmda now jon has never tasted this, the sn2 between iodo alkanes and ammonia does yeilds 90 % in ipa ...
3-9-2009 at 22:21
by: jon
Monomethylation of primary amines: N-methyl-2-phenethylamine
well have you cosidered the cesium promoted/mediated mono n-alkylation of primary amines?
or evena ...
21-8-2009 at 16:19
by: jon
Ethyl/Isopropyl Bromide preparation
you know i was wondering could this type of bromination be performed owing to the possibility of aro ...
7-7-2009 at 19:27
by: jon
phenyl-2-bromopropane from allylbenzene
do this make the hbr insitu in acetic acid. works great the only quirk is that no, you just leave it ...
7-7-2009 at 17:59
by: jon
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