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Short question / quick answer - Thread
As you might know, orgsyn.org publishes procedures tha usually provide some range of yields or maybe ...
7-2-2016 at 10:38
by: byko3y
4-alkylthio-2,5-dimethoxybenzaldehyde, Sulfuric Duff reaction
[b]laserlisa[/b], if you have some articles (at least links) that can prove your point, then I would ...
7-2-2016 at 07:25
by: byko3y
Purifying sulfuric acid
Too bad chlorine is almost insoluble in sulfuric acid.
5-2-2016 at 14:27
by: byko3y
4-alkylthio-2,5-dimethoxybenzaldehyde, Sulfuric Duff reaction
[b]laserlisa[/b], [url=https://www.erowid.org/archive/rhodium/chemistry/formylation.duff-hmta-tfa.ht ...
5-2-2016 at 12:50
by: byko3y
Purifying sulfuric acid
I was just going to post a message that I've discovered a hydrogen peroxide to clean the sulfuric ac ...
2-2-2016 at 16:50
by: byko3y
Hofmann Rearrangement of 3,4,5-trimethoxybenzamide
[b]chemrox[/b], I don't understand your question, did you want to ask something like "what is in fac ...
28-1-2016 at 08:48
by: byko3y
Hofmann Rearrangement of 3,4,5-trimethoxybenzamide
In nature there cannot exist 12,5% NaOCl solution. There can be "approx 10% solution", "I've just me ...
27-1-2016 at 06:54
by: byko3y
Collidine vs Pyridine
Dr.Bob, DMAP is more similar to pyridine than collidine/lutidine is. E.g. Dakin-West reaction gives ...
25-1-2016 at 18:41
by: byko3y
Collidine vs Pyridine
Collidine here is a 2,x,6-pyridine, and it plays a role on non-nucleophilic base for condensation re ...
25-1-2016 at 06:59
by: byko3y
Preparation of 2-aminophenol from Salicylic Acid
Just to keep all the information together:
[url=http://dx.doi.org/10.1021/ja01104a525]Polyphosphori ...
24-1-2016 at 05:26
by: byko3y
Aldehyde distillation/purification
That's because nobody actually cares in the first place. Second - there can be different scenarios o ...
23-1-2016 at 09:30
by: byko3y
Muriatic Acid
FFS, HCl is extreemely easy to purify with any simple device, while any concentration can be achieve ...
21-1-2016 at 21:33
by: byko3y
Anhydrous Aluminum Bromide
You correctly pointed that saturated hydrocarbons actually react with bromine. Once I was stupid eno ...
18-1-2016 at 15:18
by: byko3y
Anhydrous Aluminum Bromide
[color=Teal]Didn't want to create a new thread - answering to this one.[/color]
As you might know, ...
18-1-2016 at 13:04
by: byko3y
Question about tartaric acid and it's use for resolution of racemic amines
https://en.wikipedia.org/wiki/Chirality_(chemistry)
Different nomenclatures reflect different prope ...
14-1-2016 at 21:40
by: byko3y
toluene --> benzaldehyde
gsd, you are overemphasizing the problem. If you would try to use e.g. dead burnt ZnO as a catalyst ...
14-1-2016 at 09:12
by: byko3y
Benzaldehyde Assay Procedure
Some of you just forgot that 80 years ago there was no equipment $250K worth, there was no widesprea ...
12-1-2016 at 16:38
by: byko3y
Benzaldehyde Assay Procedure
Bisulfite adduct is not slightly soluble in water. It is VERY SOLUBLE in water - this is a main misc ...
11-1-2016 at 20:30
by: byko3y
Hemetsberger indole synthesis with ortho-vanillin
This article is about oligosacharides, not about benzyl phenyl ether debenzylation.
[quote]Typical ...
11-1-2016 at 20:15
by: byko3y
Purifying sulfuric acid
I've posted few times on this board instructions for sulfuric acid distillation.
- you should never ...
11-1-2016 at 17:11
by: byko3y
Hemetsberger indole synthesis with ortho-vanillin
If you wish.
11-1-2016 at 15:16
by: byko3y
Hydrochlorination of alk-1-ene?
I've had such experience. I've used silica gel as a catalyst for hydrochlorination of butene with hy ...
11-1-2016 at 15:13
by: byko3y
3 step ultra pure water
What is the application of water? A drinking water with normal salt content, or maybe a regular dist ...
9-1-2016 at 14:19
by: byko3y
Sodium Ethyl Sulfate
I think you gonna need a vacuum if you want to obtain completely ethanol-free crystals, because ethy ...
7-1-2016 at 23:52
by: byko3y
Hemetsberger indole synthesis with ortho-vanillin
clearly_not_atara, it's 2-nitro and 2-carboxylate-benzyl protecting group, not just an unsubstituted ...
7-1-2016 at 11:48
by: byko3y
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