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KCLO3 by way of H2O + KCL
Here's a bit more "guff" I put together a while back, on the running of the cell .....

One advant ...
27-3-2008 at 17:48
by: Xenoid
KCLO3 by way of H2O + KCL
Hi Dann2

No, they wore through at the level of the top of the cathode. The remaining stubs which ...
27-3-2008 at 17:02
by: Xenoid
10 litre chlorate cell
As a follow-up to my post a few months ago, earlier in this thread (see page 7), on the construction ...
26-3-2008 at 22:06
by: Xenoid
Strontium Carbonate--->Strontium Nitrate problems
Hi Cookie,

Did you use stoichiometric quantities of the reagents.

SrCO3 + 2HNO3 ---> Sr(NO3 ...
19-3-2008 at 00:43
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by Ioxoi[/i]
Second, and on topic: have you tried using K2Cr2O7 with yo ...
13-3-2008 at 17:38
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by tentacles[/i]
Perhaps your dry but unbaked coats are redissolving wh ...
8-3-2008 at 11:38
by: Xenoid
Total Failure
My latest perchlorate anode was my most sophisticated attempt to date, and utilised UMLT* and featur ...
7-3-2008 at 14:23
by: Xenoid
Physical properties of HgCO3, mercuric carbonate
Some further notes, again from Mellor's:

Mercuric chloride, (corrosive sublimate), HgCl2 was form ...
28-2-2008 at 11:27
by: Xenoid
Taking the carbon dioxide out of coal!
There is an article on CO2 sequestering in the latest New Scientist Magazine;

Crystal sponges cap ...
27-2-2008 at 15:31
by: Xenoid
Physical properties of HgCO3, mercuric carbonate
I think you are out of luck!

From my Mellor's:

"Mercuric carbonate has not been prepared, and ...
26-2-2008 at 10:59
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by dann2[/i]
Hello,

@Xenoid
I never seen that patent before. It ef ...
25-2-2008 at 18:07
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by hashashan[/i]
Why is it going to wear away? LD doesnt wear away that ...
24-2-2008 at 21:27
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
@ Rosco

I'm getting very confused with all this ... :(

For example, in the case of Hubert I pu ...
24-2-2008 at 19:55
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by tentacles[/i]
I'm planning on messing with those two oxidative soak ...
24-2-2008 at 16:49
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Well, I have given up on oxidative soak for the moment.

I oxidised some SnCl2 solution with H2O2 ...
21-2-2008 at 20:03
by: Xenoid
Ammonia + PET Bottles = Disaster
PET - what it lacks in chemical resistance, it sure makes up for with physical toughness!

I just ...
20-2-2008 at 11:50
by: Xenoid
Ammonia + PET Bottles = Disaster
A few months ago I aquired some laboratory grade ammonia solution from a local online source. When I ...
19-2-2008 at 19:45
by: Xenoid
Fe2O3
As an adjunct to what 12AX7 has said, here is some information from my Mellor's;

"Ferrous hydroxi ...
19-2-2008 at 14:12
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
Well, that last abstract "Metastannic Acid and its Compounds" is as clear as mud ....!

Both my at ...
19-2-2008 at 13:23
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by tentacles[/i]
That would leave us looking to another method for the ...
18-2-2008 at 00:39
by: Xenoid
Lithium (Per)Chlorate cell
[quote][i]Originally posted by hashashan[/i]

no perchlorate has yet formed ... [/quote]

Hashas ...
17-2-2008 at 16:57
by: Xenoid
Some Good News and Some Bad News
I have finally pulled the plug on Hubert and non-Purple Haze. They were still producing KClO3 but I ...
15-2-2008 at 17:10
by: Xenoid
gelatin as buffer
I think perhaps in this case (dyeing) the term "buffer" is being used in a more general sense compar ...
14-2-2008 at 19:45
by: Xenoid
Electrochemical ozone generation
[quote][i]Originally posted by Pulverulescent[/i]
I've posted enough details already to show this i ...
14-2-2008 at 14:42
by: Xenoid
Multilayer Metal Oxide / Titanium Anodes for Chlorate/Perchlorate
[quote][i]Originally posted by tentacles[/i]
....but at low temps (ie in my freezer!) I should get ...
13-2-2008 at 20:05
by: Xenoid
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