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Room temperature Swern
[rquote=179333&tid=13953&author=DJF90]Moffatt type oxidations are well known and I've got th ...
6-6-2010 at 17:58
by: Paddywhacker
Room temperature Swern
Thanks NI, here is [url=http://ifile.it/xc3jwuo/H%20Temp%20Swern.rar]the url.[/url]
6-6-2010 at 01:38
by: Paddywhacker
Room temperature Swern
Everyone is familiar with the famous Swern oxidation. It is a favourite in textbooks and in industr ...
5-6-2010 at 22:24
by: Paddywhacker
Martini glass SC?
You want to use a snapped-off glass in your own [i]Superior Colliculus[/i], or somebody elses? I ho ...
30-5-2010 at 00:04
by: Paddywhacker
Electrolysis of aqueous acetate salts
yes
27-5-2010 at 18:11
by: Paddywhacker
Preparation of HBF4...
I worked in a place that did this reaction many years ago. Adding powdered boric acid to HF solution ...
20-5-2010 at 21:47
by: Paddywhacker
3,4 dihydroxyphenyl ethanol (Hydroxytyrosol)
[rquote=178089&tid=13850&author=entropy51]As if you have eugenol, vanillin, diethyl sulfate, ...
19-5-2010 at 21:57
by: Paddywhacker
disposing of chloroform and hydrogen chloride
The hydrogen chloride should be neutralized first, with garden lime or with bicarbonate.

Chlorofo ...
19-5-2010 at 00:39
by: Paddywhacker
Permanganates
Yes. Next time I will mix and melt all of the hydroxides and nitrates, then add a little MnO2 and i ...
17-5-2010 at 21:16
by: Paddywhacker
Permanganates
The reaction should have produced water, causing the melt to bubble or foam vigorously.

MnO2 + 2K ...
17-5-2010 at 15:26
by: Paddywhacker
Permanganates
An equimolar amount of NaOH and KOH forms an eutectic that melts well below 200 degrees. So I tried ...
16-5-2010 at 21:43
by: Paddywhacker
question an N-acetylation of aniline, using aspirin
It seems that asprin's ability as a transacetylator is out there ...
http://www.justice.gov/dea/pr ...
12-5-2010 at 01:19
by: Paddywhacker
xylazine powder. Is artchemicals.com any good?
If it's for your cat then a vet will give you a script, or will give you better advice.

Look afte ...
10-5-2010 at 00:19
by: Paddywhacker
The short questions thread (2)
Or you can sublimate your passion for chemistry by indulging in the preparation of sublime meals.
3-5-2010 at 14:15
by: Paddywhacker
Very beginner, questions and home curriculum
Yes that sounds good. Last time I checked, a couple of years ago though, there wasn't much in chem ...
1-5-2010 at 16:28
by: Paddywhacker
Readily available Plasticizers & Binders
[rquote=176743&tid=6189&author=csm9420]...

How can i make DIOP?? can you give me any inst ...
29-4-2010 at 23:22
by: Paddywhacker
Readily available Plasticizers & Binders
Plasticizers & binders for what?

Those that you would making some bioplastic would be no good ...
28-4-2010 at 00:51
by: Paddywhacker
toluene --> benzaldehyde
For your pleasure-
24-4-2010 at 00:01
by: Paddywhacker
Column chromatography materials
Ground up kitty litter sounds like an interesting experiment.

I have 50 mesh, 100 mesh and 200 me ...
19-4-2010 at 13:31
by: Paddywhacker
Column chromatography materials
I tried to make a granulated corn-starch chromatography medium by moistening 90% corn starch + 10% p ...
19-4-2010 at 02:27
by: Paddywhacker
Camphor: Any interesting experiment?
Camphor smells nice, and you could explore that avenue, looking for interesting smells.

My idea f ...
16-4-2010 at 16:45
by: Paddywhacker
Computer in Lab protection
How about keeping it in a glovebox?

More sensibly, you could enclose the screen & computer in ...
17-3-2010 at 19:03
by: Paddywhacker
Ethyl chloride/chloroethane prep.
Dry HCl has been prepared by dropping hydrochloric acid onto a large excess of anhydrous calcium chl ...
12-2-2010 at 15:26
by: Paddywhacker
the journal of irreproducible results presents: KCN from KOH and formamide
[rquote=171476&tid=13376&author=Panache]A great source of acidic or caustic vapour is simply ...
9-2-2010 at 00:24
by: Paddywhacker
valeronitrile
That's rather a lot... more of an industrial problem than an amateur experimentalist one. I would s ...
4-2-2010 at 02:39
by: Paddywhacker
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