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Making Silver Oxide
Yes, sterling dissolves in hot concentrated sulfuric acid.
16-7-2011 at 07:34
by: Fleaker
Misuse of laboratory materials
This is horrifying. Where is the intent to harm anyone or inflict any sort of terror? The man was tr ...
15-7-2011 at 18:34
by: Fleaker
Getting gas out of N2O capsules in controlled way?
That's a rough approximation I suppose and more tuned to my thought of the economy of scale; at the ...
15-7-2011 at 18:11
by: Fleaker
Silver nitrate - green !!?? help
If you started from sterling, you can boil it with sodium formate to give you 99,99 fine silver.

...
15-7-2011 at 16:43
by: Fleaker
Making Silver Oxide
Dissolve it in hot sulfuric acid, precipitate with HCl, keeping it wet, then slurry it with a 1.2 mo ...
15-7-2011 at 16:41
by: Fleaker
Film about amateur scientist
I think Woelen would be perfect! He's as meticulous as any, exceedingly well-educated, and passionat ...
15-7-2011 at 16:38
by: Fleaker
Getting gas out of N2O capsules in controlled way?
Woelen,

Forget using the capsules. I suggest you consider the use of sulfamic acid and nitric aci ...
6-7-2011 at 18:30
by: Fleaker
Nitric acid color
Once I added RFNA to 70% nitric acid and was left with a brilliant green-blue solution. I wonder if ...
21-6-2011 at 21:05
by: Fleaker
how many females here
[rquote=213618&tid=16734&author=iHME]I once met a female with a keen interest in HE's. Very ...
21-6-2011 at 20:42
by: Fleaker
Reaction between NH4OH and Al2O3
What reaction?


Al2O3 has different modifications. Some are easier to digest than others. Ammoni ...
21-6-2011 at 20:41
by: Fleaker
Puirifying gold from old jewelry
If you are taking gold from jewelery and want it to be of 4N purity for use in your experiments, the ...
21-6-2011 at 20:37
by: Fleaker
Metal prices on ebay.
The indium-gallium eutectic is liquid at room temperature, and while an order of magnitude more expe ...
12-6-2011 at 19:20
by: Fleaker
US Carcinogen list gets additions
As a scientist, I think his claims deserve some study.

:P

Too bad it's not in JAMA...that'd b ...
12-6-2011 at 19:05
by: Fleaker
Metal prices on ebay.
What the hell do you want with all that cadmium?

12-6-2011 at 19:03
by: Fleaker
The Synthesis of Sulfur Trioxide and Oleum: the vanadium (V) oxide-catalyzed method
Hey all!

I'm glad to see someone finally going for it! Any questions, ask! I made a few modificat ...
12-6-2011 at 19:01
by: Fleaker
Metal prices on ebay.
It's just CsCl, there are no shipping restrictions. It's just a saltier tasting salt than table salt ...
12-6-2011 at 18:41
by: Fleaker
Ways to Bromine (or HBr) from KBr
The absolute best way to make bromine (if you have the reagents) is from potassium bromide, potassiu ...
12-6-2011 at 18:35
by: Fleaker
Anyone interested in buying some zirconium?
The alkali metal is distilled off, and it's supposedly better than Ca for making gas free metal.
24-4-2011 at 07:26
by: Fleaker
Extraction of platinum metal from Sperrylite (PtAs2)
Well said Neil. He can even afford to pay the 3X over spot that 5N zone refined platinum commands (a ...
24-4-2011 at 07:23
by: Fleaker
Anyone interested in buying some zirconium?
Oh, I don't really care about broken filaments. I merely wanted it for making Cs from its dichromate ...
23-4-2011 at 09:08
by: Fleaker
Anyone interested in buying some zirconium?
How much would a kilogram of swarf be?

23-4-2011 at 08:59
by: Fleaker
platinum coated mesh/wool
You can at least try it. I know it works for hydrogenations.
23-4-2011 at 08:54
by: Fleaker
Extraction of platinum metal from Sperrylite (PtAs2)
I'd really wish he'd just desist. This is very dangerous to do and is NOT for someone with no experi ...
23-4-2011 at 08:53
by: Fleaker
Extraction of platinum metal from Sperrylite (PtAs2)
Are you in North America? I know multiple parties that would be interested in buying.
22-4-2011 at 05:58
by: Fleaker
Anyone interested in buying some zirconium?
These prices are much lower than that available from Alfa, Goodfellow, and Advent RM.

Unfortunat ...
20-4-2011 at 08:40
by: Fleaker
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