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Pentryl
Theres a problem with the need for a solvent to condense the solid polyols with DNCB, any ideas on t ...
25-4-2007 at 00:49
by: Axt
Pentryl
Sounds like a mixup to me dichlorobenzene <-> dinitrochlorobenzene.. though it'd be nice if it ...
23-4-2007 at 06:29
by: Axt
Silver Fulminate Synthesis
[quote][i]Originally posted by ssdd[/i]

I let the beaker with the Blue/White solution sit overnig ...
19-4-2007 at 09:56
by: Axt
Cyclohexanone peroxide
If cyclohexanone bears any analogy to that of cyclopentanone and I expect that it does, treating it ...
18-4-2007 at 03:24
by: Axt
Silver Fulminate Synthesis
Adding ethanol would probably have precipitated some of the AgNO3 formed via dissolving the Ag in HN ...
15-4-2007 at 07:51
by: Axt
Silver Fulminate Synthesis
You left it too cold. Fulminates are hot and ugly reactions. See the attachment for what seems to be ...
15-4-2007 at 07:16
by: Axt
Azides
Your after US patent #3155456 "Process for Preparing Hydrazinium Azide" Attached, Reflux hydrazine s ...
15-4-2007 at 04:04
by: Axt
Diisonitrosoacetone
Interesting, pity it doesn't provide any details in the ber. article. And about the reaction rate, m ...
13-4-2007 at 20:11
by: Axt
Diisonitrosoacetone
This one from Berichte der Deutschen chemischen Gesellschaft, Cant read it but supposedly holds the ...
11-4-2007 at 01:53
by: Axt
Diisonitrosoacetone
I'm attaching the two references given in Org Synth, The first from J. Chem. soc is quicker then the ...
11-4-2007 at 01:50
by: Axt
Trinitromelamine
The direct nitration of melamine produces dinitroammeline aka 4,6-Dinitramino-1,3,5-triazine-2(1H)- ...
7-4-2007 at 21:39
by: Axt
Trinitromelamine
[quote][i]Extract from Ind. Eng. Chem: 33(6); 770[/i]

<b>Methylolmelamines</b>. Mela ...
3-4-2007 at 22:30
by: Axt
Diisonitrosoacetone
Benzotrifuroxan has been well studied, and far exceeds tetryl in performance. Its performance is sli ...
2-4-2007 at 20:48
by: Axt
Diisonitrosoacetone
Heres the extracts showing examples of aromatic nitrolic acids to furoxan and trinitromethanes.

[Ed ...
1-4-2007 at 19:32
by: Axt
Diisonitrosoacetone
If diisonitrosoacetone was to condense with hydroxylamine to produce trioximinopropane it seems like ...
1-4-2007 at 19:27
by: Axt
Pentryl
[quote]<u>Picric acid</u>: By reacting with sodium hydroxide in methanol, then nitration ...
26-3-2007 at 21:53
by: Axt
Pentryl
Journal references used.


Edit: uploading or file size problems.. grrrr

Heres some of them

[ ...
26-2-2007 at 22:00
by: Axt
Pentryl
@ Davstar: In defence of pentryl, it was pressed to a much lower density then the PETN in the detona ...
26-2-2007 at 21:33
by: Axt
Pentryl
<center><font size="10">Pentryl</font>
<font size="5">(Trinitrophenylnitram ...
23-2-2007 at 19:45
by: Axt
Unconventional Shaped Charges
[quote][i]Originally posted by Axt[/i]
Though there is the book, "Evaluation of Improvised Shaped C ...
16-1-2007 at 21:06
by: Axt
PETN-based Cast Explosives
[quote][i]Originally posted by Nitrojet[/i]
I made several ball drop tests in a simple apparatus w ...
1-12-2006 at 01:44
by: Axt
Glyoxime, Diaminofurazan and Some Energetic Derivatives
[quote][i]Originally posted by NUKE[/i]
I have one question. Can i use 30% H2O2 instead of 50% H2O2 ...
20-11-2006 at 21:17
by: Axt
Exotic thermites & analogs
[quote][i]Originally posted by nitro-genes[/i]
With liquid water instead of ice the results wouldn ...
20-11-2006 at 16:59
by: Axt
Vacuum Distillation of H2O2
Extract from PATR2700 H219:

<i>Explosive and Combustion Props</i>: Pure H2O2 is readi ...
14-11-2006 at 12:49
by: Axt
Nitration of Tris????
[quote]It seems to me that getting the free amine from the unstable salt shouldnt be too difficult.[ ...
9-11-2006 at 01:59
by: Axt
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