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Learning to respect NBS the hard way Sauron: Yes, of course it was my fault. First and foremost because I did not take the necessary safe ... |
27-11-2007 at 02:44 by: jam640 |
Learning to respect NBS the hard way I have attached the full article now.
And it actually gives a caution of the reaction between NIS a ... |
26-11-2007 at 05:37 by: jam640 |
Learning to respect NBS the hard way Sorry Sauron, I didn't have SciFinder access when I looked it up earlier today so I just did hasty G ... |
26-11-2007 at 05:32 by: jam640 |
Learning to respect NBS the hard way Sauron: No, it was not a direct scale-up of solvents but an apparently somewhat optimistic estimatio ... |
26-11-2007 at 04:45 by: jam640 |
Learning to respect NBS the hard way Yes, I don't know. It just strikes me as very odd that the reaction had been going with slight heati ... |
26-11-2007 at 02:59 by: jam640 |
Learning to respect NBS the hard way Yes, I agree with both.
Accidents and chemistry go hand in hand, although you should always take th ... |
26-11-2007 at 01:45 by: jam640 |
Learning to respect NBS the hard way It was butyrophenone.
From an reference (I can look it up later) which said diethyl ether worked be ... |
25-11-2007 at 00:07 by: jam640 |
Learning to respect NBS the hard way Thank you, I'm calmer now.
I really appreciate your posts.
You just get so paranoid and panicy ... |
24-11-2007 at 13:41 by: jam640 |
Learning to respect NBS the hard way I would really really appreciate an prompt reply if anyone has knowledge of the compound in question ... |
24-11-2007 at 13:11 by: jam640 |
Learning to respect NBS the hard way I'm getting a bit paranoid about the health effects.
I inhaled some, of course.
It was butyropheno ... |
24-11-2007 at 12:09 by: jam640 |
Learning to respect NBS the hard way The funny thing is that the reaction stampeded after several hours, after I had turned of the heatin ... |
24-11-2007 at 10:45 by: jam640 |
Learning to respect NBS the hard way Oh boy.
I'm still kinda shaking.
I decided to do a reaction I'd wanted to do for a long time to ... |
24-11-2007 at 10:43 by: jam640 |
1,3,5-Tris-(4-carboxyphenyl)benzene, please help!!! Yes, organolithiums tend to be _very_ sensitive to oxygen/water contant and slightest impurity may f ... |
15-11-2007 at 14:01 by: jam640 |
1,3,5-Tris-(4-carboxyphenyl)benzene, please help!!! Probably according to Journal of the American Chemical Society, 126(3), 884-890; 2004.
1. Is your i ... |
15-11-2007 at 02:59 by: jam640 |
Flammable limits and safety of diethyl ether No, of course the fume concentration would be very much higher closer to the source but in _theory_ ... |
7-11-2007 at 12:33 by: jam640 |
Flammable limits and safety of diethyl ether I was curious on how much diethyl ether gas that had to be present for a flammable/explosive mixture ... |
7-11-2007 at 03:46 by: jam640 |
Storage of Di-ethylether I remember when I started studying chemistry how scared I was of using diethyl ether due to the pero ... |
5-11-2007 at 07:01 by: jam640 |
is 2,5-dimethoxyphenyl-2-nitroethane a white solid at r.t.? Yes, most likely boron salts. They have a tendency to precipitate after a while unless extensive car ... |
29-10-2007 at 10:09 by: jam640 |
2-bromonaphthalene from naphthalene freepatentsonline have a bit confusing website layout. I do not know if you really have a problem or ... |
23-10-2007 at 03:18 by: jam640 |
achiral molecules and chiral crystals If you have access to Cambridge Structural Database you may do a search for compounds that crystalli ... |
22-10-2007 at 07:35 by: jam640 |
Need Pd/C, Thionyl Chloride, V, Ir, Pt etc... The level of maturity has really sunken to a new low on this board lately...
Can't the people who d ... |
22-10-2007 at 00:23 by: jam640 |
predicting degree of unsaturation The degree of unsaturation is a very simplified way of calculating the amount of multiple bonds pres ... |
21-10-2007 at 00:04 by: jam640 |
carboxylic acid functional group Carbonic acid is carbon dioxide dissolved in water.
And that is not a mechanism, but a chemical equ ... |
18-10-2007 at 09:17 by: jam640 |
Solubility of NBS and succinimide in diethyl ether Because I am not at the laboratory (late night here), and I am an impatient bastard who likes to rid ... |
17-10-2007 at 10:07 by: jam640 |
Solubility of NBS and succinimide in diethyl ether Does anyone have empirical data on the solubility of n-bromosuccinimide and succinimide in diethyl e ... |
17-10-2007 at 09:48 by: jam640 |
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