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Chemistry behind RDX
When I have made RDX I have always performed the nitrolysis then after addition is complete, allow i ... |
13-7-2024 at 10:10
by: greenlight |
Chemistry behind RDX
[rquote=693924&tid=150602&author=ManyInterests][rquote=693912&tid=150602&author=gree ... |
9-7-2024 at 10:55
by: greenlight |
LL8 from Dr. Liptakov
[rquote=694033&tid=158259&author=Laboratory of Liptakov]Just a due to sesitivity and unstabi ... |
9-7-2024 at 10:42
by: greenlight |
Rubidium Chlorate
Pretty cool stuff
You can use a methylene blue test for presence of perchlorate if you have, a ... |
9-7-2024 at 10:20
by: greenlight |
Chemistry behind RDX
[rquote=693905&tid=150602&author=ManyInterests]Decided to bump this up since I have been wor ... |
30-6-2024 at 18:59
by: greenlight |
Acetic anhydride preparation
[rquote=693492&tid=9&author=Keras]So today I've tried AcOH in DMSO + phosphorus pentoxide.
... |
30-6-2024 at 09:30
by: greenlight |
Can a perchlorate cell go wrong?
Great sign, you got perchlorate
It's always difficult with the perc cell because the product do ... |
29-6-2024 at 19:44
by: greenlight |
Separating Toluene from N-Butyl Acetate
Its not really a complex mixture, you have a difference in boiling point of 16°C. The 300mm vigreu ... |
29-6-2024 at 19:20
by: greenlight |
Can a perchlorate cell go wrong?
Have you done a test for the presence of perchlorate. I believe methylene blue was the one to use a ... |
29-6-2024 at 10:43
by: greenlight |
Separating Toluene from N-Butyl Acetate
You could use the allihn as a column without water circulating through it and pack it with broken gl ... |
29-6-2024 at 10:16
by: greenlight |
Separating Toluene from N-Butyl Acetate
How long is your column?
You could pack it with broken glass pieces for extra surface area for co ... |
29-6-2024 at 06:24
by: greenlight |
Nitric acid from calcium nitrate
You could also convert the calcium nitrate to potassium nitrate with potassium chloride if that's ea ... |
15-6-2024 at 09:33
by: greenlight |
Det cap questions: e-match nichrome, selecting a primary
I'm still a fan of aluminium cased caps filled with 700mg recrystallised, pressed PETN base charge, ... |
15-6-2024 at 09:24
by: greenlight |
Acetic anhydride preparation
@paulll, yes, stoichiometrically the yields from phosphorus pentoxide reagent are terrible haha. I ... |
27-5-2024 at 08:51
by: greenlight |
Acetic anhydride preparation
Thankyou for the replies,
Would it be possible to run the reaction by slowly dripping glacial acet ... |
26-5-2024 at 09:58
by: greenlight |
Acetic anhydride preparation
Has anyone on here had any success with the reaction of phosphorus pentoxide and glacial acetic acid ... |
22-5-2024 at 10:11
by: greenlight |
Life after detonation
The right hand came out brilliantly compared to the first photo.
I always remember your accident ... |
19-5-2024 at 10:17
by: greenlight |
Pretty Pictures (2)
Some Cesium nitrate precipitating crystals out of solution as the water evaporates slowly.
[Edited ... |
8-2-2024 at 04:01
by: greenlight |
Concentrating Sulfuric Acid through Boiling
If you have a pure solution of sulfuric acid in water at a low concentration then there are two obse ... |
5-12-2023 at 02:57
by: greenlight |
Short question / quick answer - Thread
How have you stored the polyisobutylene? Away from heat, moisture and direct sunlight?
The only thi ... |
1-12-2023 at 06:09
by: greenlight |
Using a vacuum filtration flask in vacuum distillation?
[rquote=685545&tid=159668&author=Texium] I wouldn’t consider IKA to be reliable. Their dev ... |
11-7-2023 at 18:27
by: greenlight |
Using a vacuum filtration flask in vacuum distillation?
If your looking reasonably priced there is plenty of cheap chinese models on ebay but these can be p ... |
10-7-2023 at 01:36
by: greenlight |
Cocrystalization
"I dunno if cocrystalized liquids with solids like EGDN and PETN after cocrystalization the evapora ... |
7-7-2023 at 11:21
by: greenlight |
Cocrystalization
It seems there is a larger proportion of CL-20 to HMX is the usual ratio to create the cocrystal str ... |
6-7-2023 at 20:14
by: greenlight |
Chemistry behind RDX
[rquote=680432&tid=150602&author=ManyInterests]On second thought (I cannot edit my message f ... |
16-1-2023 at 10:46
by: greenlight |
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