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POCl3 via P2O5 + NaCl in borosilicate glass? Has anybody prepared phosphoryl chloride via the following method? I found it within a small-scale r ... |
16-7-2021 at 12:06 by: Opylation |
Copper hydride as a reducing agent? That’s interesting. If copper hydride is easily made then maybe the borohydride could be prepared ... |
20-6-2021 at 04:35 by: Opylation |
Interesting hydrodechlorination of PCE to (edit) dichloroethylene Hello all, on my search for a neat chloral procedure for its use in preparing trichloroacetic acid I ... |
20-6-2021 at 04:30 by: Opylation |
Forming oxalte salts of amines I know this is an old thread, but I found the conversation intriguing and wanted to add a little bit ... |
16-6-2021 at 17:11 by: Opylation |
Sythesis proposal for preparing 1,3-benzodioxole oxidation products using simple precursors If you’re looking for a phenolic dealkylation procedure then take a look at this paper. The most O ... |
14-6-2021 at 21:13 by: Opylation |
Oxalyl Chloride Challenge Off topic… removed for irrelevance
[Edited on 10-6-2021 by Opylation] |
9-6-2021 at 17:44 by: Opylation |
Oxalyl Chloride Challenge I would like to post one more paper, a parent actually, that describes the preparation on oxalyl chl ... |
8-6-2021 at 16:29 by: Opylation |
Oxalyl Chloride Challenge Liquid bromine and Oxalic acid react to form hypobromic acid, carbon monoxide and carbon dioxide. Hy ... |
8-6-2021 at 01:58 by: Opylation |
Oxalyl Chloride Challenge Just would like to provide an update that I have found a patent on the preparation of tetrachloroeth ... |
8-6-2021 at 01:12 by: Opylation |
Carbon disulfide synthesis (alternative routes) I’m not quite sure. I haven’t performed this reaction but have logged it for when I have time to ... |
6-6-2021 at 03:15 by: Opylation |
Acetaldehyde synthesis [rquote=659047&tid=55&author=EverythingAl2O3]Have we also considered the Corey-Kim oxidation ... |
5-6-2021 at 19:32 by: Opylation |
Preparation of dimethyl carbonate without autoclave or phosgene If your goal is to truly prepare dimethyl carbonate I have no tips or tricks to give. But I do want ... |
5-6-2021 at 13:43 by: Opylation |
Carbon disulfide synthesis (alternative routes) Ammonia and Carbon Disulfide react to form ammonium thiocyanate and hydrogen sulfide. However, what ... |
5-6-2021 at 00:30 by: Opylation |
toluene --> benzaldehyde I don't have any experience going through the procedure, but the salicylaldehyde synthesis via pheno ... |
4-6-2021 at 14:55 by: Opylation |
Carbon disulfide synthesis (alternative routes) [rquote=661017&tid=147199&author=garphield]Cyanamide will react with hydrogen sulfide to gen ... |
4-6-2021 at 10:49 by: Opylation |
toluene --> benzaldehyde This isn’t toluene, but phenol (made easily from salicylic acid) can be reacted with chloroform an ... |
4-6-2021 at 10:15 by: Opylation |
Oxalyl Chloride Challenge I found a paper on cyclic oxalate ester formation and properties. It looks like ethylene oxalate has ... |
4-6-2021 at 09:49 by: Opylation |
Preparation of dimethylamine I would just like to mention, “2,4-D” is an herbicide readily sold in hardware stores in the US ... |
4-6-2021 at 08:53 by: Opylation |
Oxalyl Chloride Challenge I was just thinking back to the ethylene carbonate -> chlorination -> oxalyl chloride + phosge ... |
3-6-2021 at 18:48 by: Opylation |
Cicada fungi I believe psilocin when shielded from light and oxygen can last a relatively long time compared to w ... |
3-6-2021 at 18:11 by: Opylation |
Cicada fungi “What’s wrong? Fungus got your nethers?”
That’s super interesting though. I wonder if it ... |
3-6-2021 at 12:45 by: Opylation |
Retrofinkelstein reaction (baseless inquiry) I was referring to 1.2-dichloroethane. I was under the impression that ethylene glycol + HCl makes e ... |
3-6-2021 at 01:33 by: Opylation |
Retrofinkelstein reaction (baseless inquiry) So, let me start this by saying my mind wonders when thinking of solutions to unasked questions. I w ... |
2-6-2021 at 23:59 by: Opylation |
Pyridine hydrogenation - methods? Here's a couple different sources I had logged away for the reduction of pyridine and substituted py ... |
23-5-2021 at 13:29 by: Opylation |
Oxalyl Chloride Challenge [rquote=660556&tid=82462&author=clearly_not_atara]BzCl + H2C2O4 >> BzOH + CO2 + CO + H ... |
22-5-2021 at 19:57 by: Opylation |
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